2-Aminoterephthalic acid dimethyl ester

Single crystals of the title compound, C(10)H(11)NO(4), an inter­mediate in the industrial synthesis of yellow azo pigments, were obtained from the industrial production. The mol­ecules crystallize as centrosymmetic dimers connected by two symmetry-related N—H⋯O=C hydrogen bonds. Each mol­ecule also...

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Detalles Bibliográficos
Autores principales: Brüning, Jürgen, Bats, Jan W., Schmidt, Martin U.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970453/
https://www.ncbi.nlm.nih.gov/pubmed/21577922
http://dx.doi.org/10.1107/S1600536809036095
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author Brüning, Jürgen
Bats, Jan W.
Schmidt, Martin U.
author_facet Brüning, Jürgen
Bats, Jan W.
Schmidt, Martin U.
author_sort Brüning, Jürgen
collection PubMed
description Single crystals of the title compound, C(10)H(11)NO(4), an inter­mediate in the industrial synthesis of yellow azo pigments, were obtained from the industrial production. The mol­ecules crystallize as centrosymmetic dimers connected by two symmetry-related N—H⋯O=C hydrogen bonds. Each mol­ecule also contains an intra­molecular N—H⋯O=C hydrogen bond. The dimers form stacks along the a-axis direction. Neighbouring stacks are arranged into a herringbone structure.
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spelling pubmed-29704532010-12-30 2-Aminoterephthalic acid dimethyl ester Brüning, Jürgen Bats, Jan W. Schmidt, Martin U. Acta Crystallogr Sect E Struct Rep Online Organic Papers Single crystals of the title compound, C(10)H(11)NO(4), an inter­mediate in the industrial synthesis of yellow azo pigments, were obtained from the industrial production. The mol­ecules crystallize as centrosymmetic dimers connected by two symmetry-related N—H⋯O=C hydrogen bonds. Each mol­ecule also contains an intra­molecular N—H⋯O=C hydrogen bond. The dimers form stacks along the a-axis direction. Neighbouring stacks are arranged into a herringbone structure. International Union of Crystallography 2009-09-16 /pmc/articles/PMC2970453/ /pubmed/21577922 http://dx.doi.org/10.1107/S1600536809036095 Text en © Brüning et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Brüning, Jürgen
Bats, Jan W.
Schmidt, Martin U.
2-Aminoterephthalic acid dimethyl ester
title 2-Aminoterephthalic acid dimethyl ester
title_full 2-Aminoterephthalic acid dimethyl ester
title_fullStr 2-Aminoterephthalic acid dimethyl ester
title_full_unstemmed 2-Aminoterephthalic acid dimethyl ester
title_short 2-Aminoterephthalic acid dimethyl ester
title_sort 2-aminoterephthalic acid dimethyl ester
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970453/
https://www.ncbi.nlm.nih.gov/pubmed/21577922
http://dx.doi.org/10.1107/S1600536809036095
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AT batsjanw 2aminoterephthalicaciddimethylester
AT schmidtmartinu 2aminoterephthalicaciddimethylester

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