1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea

The title compound, C(12)H(9)BrN(2)OS(2), consists of two planar parts, viz. the thio­phene ring including all substituents (r.m.s. deviation 0.007 Å) and the benzene ring including the respective substituents as well as the thione group (r.m.s. deviation 0.05 Å). The inter­planar angle is 18.84 (6)...

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Detalles Bibliográficos
Autores principales: Saeed, Sohail, Rashid, Naghmana, Hussain, Rizwan, Jones, Peter G.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970465/
https://www.ncbi.nlm.nih.gov/pubmed/21578006
http://dx.doi.org/10.1107/S1600536809038537
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author Saeed, Sohail
Rashid, Naghmana
Hussain, Rizwan
Jones, Peter G.
author_facet Saeed, Sohail
Rashid, Naghmana
Hussain, Rizwan
Jones, Peter G.
author_sort Saeed, Sohail
collection PubMed
description The title compound, C(12)H(9)BrN(2)OS(2), consists of two planar parts, viz. the thio­phene ring including all substituents (r.m.s. deviation 0.007 Å) and the benzene ring including the respective substituents as well as the thione group (r.m.s. deviation 0.05 Å). The inter­planar angle is 18.84 (6)°. An intra­molecular C(phen­yl)—N—H⋯OC hydrogen bond is observed. The three-dimensional packing involves three types of inter­actions, viz. N—H⋯S, C—H⋯S (× 2) and Br⋯S [3.6924 (6) Å].
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spelling pubmed-29704652010-12-30 1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea Saeed, Sohail Rashid, Naghmana Hussain, Rizwan Jones, Peter G. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(9)BrN(2)OS(2), consists of two planar parts, viz. the thio­phene ring including all substituents (r.m.s. deviation 0.007 Å) and the benzene ring including the respective substituents as well as the thione group (r.m.s. deviation 0.05 Å). The inter­planar angle is 18.84 (6)°. An intra­molecular C(phen­yl)—N—H⋯OC hydrogen bond is observed. The three-dimensional packing involves three types of inter­actions, viz. N—H⋯S, C—H⋯S (× 2) and Br⋯S [3.6924 (6) Å]. International Union of Crystallography 2009-09-30 /pmc/articles/PMC2970465/ /pubmed/21578006 http://dx.doi.org/10.1107/S1600536809038537 Text en © Saeed et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Saeed, Sohail
Rashid, Naghmana
Hussain, Rizwan
Jones, Peter G.
1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
title 1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
title_full 1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
title_fullStr 1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
title_full_unstemmed 1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
title_short 1-(4-Bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
title_sort 1-(4-bromo­phen­yl)-3-(2-thienylcarbon­yl)thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970465/
https://www.ncbi.nlm.nih.gov/pubmed/21578006
http://dx.doi.org/10.1107/S1600536809038537
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AT hussainrizwan 14bromophenyl32thienylcarbonylthiourea
AT jonespeterg 14bromophenyl32thienylcarbonylthiourea

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