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4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate
The hydrothermal reaction of benzene-1,4-dicarboxylic acid and 4,4′-trimethylene dipiperidine leads to the formation of the title compound, C(13)H(28)N(2) (2+)·C(8)H(4)O(4) (2−). The anion is located on a center of inversion whereas the cation is positioned on a twofold rotation axis. In the cryst...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2009
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970973/ https://www.ncbi.nlm.nih.gov/pubmed/21578413 http://dx.doi.org/10.1107/S1600536809042901 |
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author | Tseng, Feng-Shuen Lin, Chia-Her |
author_facet | Tseng, Feng-Shuen Lin, Chia-Her |
author_sort | Tseng, Feng-Shuen |
collection | PubMed |
description | The hydrothermal reaction of benzene-1,4-dicarboxylic acid and 4,4′-trimethylene dipiperidine leads to the formation of the title compound, C(13)H(28)N(2) (2+)·C(8)H(4)O(4) (2−). The anion is located on a center of inversion whereas the cation is positioned on a twofold rotation axis. In the crystal structure, the anions and cations are linked by N—H⋯O and N—H⋯(O,O) hydrogen bonds. |
format | Text |
id | pubmed-2970973 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29709732010-12-30 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate Tseng, Feng-Shuen Lin, Chia-Her Acta Crystallogr Sect E Struct Rep Online Organic Papers The hydrothermal reaction of benzene-1,4-dicarboxylic acid and 4,4′-trimethylene dipiperidine leads to the formation of the title compound, C(13)H(28)N(2) (2+)·C(8)H(4)O(4) (2−). The anion is located on a center of inversion whereas the cation is positioned on a twofold rotation axis. In the crystal structure, the anions and cations are linked by N—H⋯O and N—H⋯(O,O) hydrogen bonds. International Union of Crystallography 2009-10-23 /pmc/articles/PMC2970973/ /pubmed/21578413 http://dx.doi.org/10.1107/S1600536809042901 Text en © Tseng and Lin 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Tseng, Feng-Shuen Lin, Chia-Her 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
title | 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
title_full | 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
title_fullStr | 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
title_full_unstemmed | 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
title_short | 4,4′-Trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
title_sort | 4,4′-trimethylenedipiperidiniumbenzene-1,4-dicarboxylate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970973/ https://www.ncbi.nlm.nih.gov/pubmed/21578413 http://dx.doi.org/10.1107/S1600536809042901 |
work_keys_str_mv | AT tsengfengshuen 44trimethylenedipiperidiniumbenzene14dicarboxylate AT linchiaher 44trimethylenedipiperidiniumbenzene14dicarboxylate |