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N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide
In the title compound, C(15)H(14)N(2)O(3), the phenyl ring is disordered over two set of sites with an occupancy ratio of 0.810 (3):0.190 (3); the dihedral angle between the two components is 72.3 (4)°. The benzene and phenyl rings are oriented at dihedral angles of 69.18 (8) and 26.0 (5)° (major an...
| Autores principales: | , , , , |
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| Formato: | Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2009
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970999/ https://www.ncbi.nlm.nih.gov/pubmed/21578480 http://dx.doi.org/10.1107/S1600536809044122 |
| _version_ | 1782190522181353472 |
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| author | Shafiq, Zahid Yaqub, Muhammad Tahir, M. Nawaz Hussain, Abid Iqbal, M. Saeed |
| author_facet | Shafiq, Zahid Yaqub, Muhammad Tahir, M. Nawaz Hussain, Abid Iqbal, M. Saeed |
| author_sort | Shafiq, Zahid |
| collection | PubMed |
| description | In the title compound, C(15)H(14)N(2)O(3), the phenyl ring is disordered over two set of sites with an occupancy ratio of 0.810 (3):0.190 (3); the dihedral angle between the two components is 72.3 (4)°. The benzene and phenyl rings are oriented at dihedral angles of 69.18 (8) and 26.0 (5)° (major and minor orientations, respectively), and an intramolecular O—H⋯O hydrogen bond occurs. In the crystal, molecules are linked by N—H⋯O, O—H⋯O and C—H⋯O interactions, generating a three-dimensional network. |
| format | Text |
| id | pubmed-2970999 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2009 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-29709992010-12-30 N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide Shafiq, Zahid Yaqub, Muhammad Tahir, M. Nawaz Hussain, Abid Iqbal, M. Saeed Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(14)N(2)O(3), the phenyl ring is disordered over two set of sites with an occupancy ratio of 0.810 (3):0.190 (3); the dihedral angle between the two components is 72.3 (4)°. The benzene and phenyl rings are oriented at dihedral angles of 69.18 (8) and 26.0 (5)° (major and minor orientations, respectively), and an intramolecular O—H⋯O hydrogen bond occurs. In the crystal, molecules are linked by N—H⋯O, O—H⋯O and C—H⋯O interactions, generating a three-dimensional network. International Union of Crystallography 2009-10-28 /pmc/articles/PMC2970999/ /pubmed/21578480 http://dx.doi.org/10.1107/S1600536809044122 Text en © Shafiq et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Shafiq, Zahid Yaqub, Muhammad Tahir, M. Nawaz Hussain, Abid Iqbal, M. Saeed N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide |
| title |
N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide |
| title_full |
N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide |
| title_fullStr |
N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide |
| title_full_unstemmed |
N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide |
| title_short |
N′-[(E)-4-Hydroxy-3-methoxybenzylidene]benzohydrazide |
| title_sort | n′-[(e)-4-hydroxy-3-methoxybenzylidene]benzohydrazide |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970999/ https://www.ncbi.nlm.nih.gov/pubmed/21578480 http://dx.doi.org/10.1107/S1600536809044122 |
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