1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide

The title compound, C(17)H(19)N(3)O(3)S, crystallizes with two closely similar independent mol­ecules related by a pseudotranslation of c/2. Each mol­ecule consists of three approximately planar moieties centred on the N(2)CS group and the two ring systems. The packing involves classical H bonds of...

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Detalles Bibliográficos
Autores principales: Khanum, Saira, Farman, Muhammad, Rama, Nasim H., Hameed, Shahid, Jones, Peter G.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971009/
https://www.ncbi.nlm.nih.gov/pubmed/21578223
http://dx.doi.org/10.1107/S1600536809036599
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author Khanum, Saira
Farman, Muhammad
Rama, Nasim H.
Hameed, Shahid
Jones, Peter G.
author_facet Khanum, Saira
Farman, Muhammad
Rama, Nasim H.
Hameed, Shahid
Jones, Peter G.
author_sort Khanum, Saira
collection PubMed
description The title compound, C(17)H(19)N(3)O(3)S, crystallizes with two closely similar independent mol­ecules related by a pseudotranslation of c/2. Each mol­ecule consists of three approximately planar moieties centred on the N(2)CS group and the two ring systems. The packing involves classical H bonds of the form N(amide)—H⋯S and N(hydrazine)—H⋯OC, together with various weak hydrogen bonds and N(hydrazine)—H⋯π inter­actions. The overall packing is three-dimensional, but layer substructures parallel to the xz plane can be readily identified. Each mol­ecule forms a topologically equivalent set of hydrogen-bond inter­actions.
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spelling pubmed-29710092010-12-30 1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide Khanum, Saira Farman, Muhammad Rama, Nasim H. Hameed, Shahid Jones, Peter G. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(19)N(3)O(3)S, crystallizes with two closely similar independent mol­ecules related by a pseudotranslation of c/2. Each mol­ecule consists of three approximately planar moieties centred on the N(2)CS group and the two ring systems. The packing involves classical H bonds of the form N(amide)—H⋯S and N(hydrazine)—H⋯OC, together with various weak hydrogen bonds and N(hydrazine)—H⋯π inter­actions. The overall packing is three-dimensional, but layer substructures parallel to the xz plane can be readily identified. Each mol­ecule forms a topologically equivalent set of hydrogen-bond inter­actions. International Union of Crystallography 2009-10-03 /pmc/articles/PMC2971009/ /pubmed/21578223 http://dx.doi.org/10.1107/S1600536809036599 Text en © Khanum et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Khanum, Saira
Farman, Muhammad
Rama, Nasim H.
Hameed, Shahid
Jones, Peter G.
1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
title 1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
title_full 1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
title_fullStr 1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
title_full_unstemmed 1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
title_short 1-(4-Ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
title_sort 1-(4-ethoxy­benzo­yl)-4-(4-methoxy­phen­yl)thiosemicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971009/
https://www.ncbi.nlm.nih.gov/pubmed/21578223
http://dx.doi.org/10.1107/S1600536809036599
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AT hameedshahid 14ethoxybenzoyl44methoxyphenylthiosemicarbazide
AT jonespeterg 14ethoxybenzoyl44methoxyphenylthiosemicarbazide

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