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(3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
The title compound, C(29)H(28)O(9), was isolated from the reaction of 4,6-dimethoxy-2-(4-methoxyphenyl)-3-benzofuran and α-methoxycarbonylcinnaminate. The two aromatic rings form a dihedral angle of 22.7 (1)°. One methoxycarbonyl group is disordered between two orientations in a 0.612 (4):0.38...
Autores principales: | , , , |
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971057/ https://www.ncbi.nlm.nih.gov/pubmed/21578476 http://dx.doi.org/10.1107/S1600536809042196 |
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author | Wang, Xian-You Li, Nan Ma, Yong-Qiang Qin, Zhao-Hai |
author_facet | Wang, Xian-You Li, Nan Ma, Yong-Qiang Qin, Zhao-Hai |
author_sort | Wang, Xian-You |
collection | PubMed |
description | The title compound, C(29)H(28)O(9), was isolated from the reaction of 4,6-dimethoxy-2-(4-methoxyphenyl)-3-benzofuran and α-methoxycarbonylcinnaminate. The two aromatic rings form a dihedral angle of 22.7 (1)°. One methoxycarbonyl group is disordered between two orientations in a 0.612 (4):0.388 (4) ratio. The crystal structure exhibits no significantly short intermolecular contacts. |
format | Text |
id | pubmed-2971057 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29710572010-12-30 (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate Wang, Xian-You Li, Nan Ma, Yong-Qiang Qin, Zhao-Hai Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(29)H(28)O(9), was isolated from the reaction of 4,6-dimethoxy-2-(4-methoxyphenyl)-3-benzofuran and α-methoxycarbonylcinnaminate. The two aromatic rings form a dihedral angle of 22.7 (1)°. One methoxycarbonyl group is disordered between two orientations in a 0.612 (4):0.388 (4) ratio. The crystal structure exhibits no significantly short intermolecular contacts. International Union of Crystallography 2009-10-28 /pmc/articles/PMC2971057/ /pubmed/21578476 http://dx.doi.org/10.1107/S1600536809042196 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Wang, Xian-You Li, Nan Ma, Yong-Qiang Qin, Zhao-Hai (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
title | (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
title_full | (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
title_fullStr | (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
title_full_unstemmed | (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
title_short | (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
title_sort | (3r*)-methyl 3-[(2s*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971057/ https://www.ncbi.nlm.nih.gov/pubmed/21578476 http://dx.doi.org/10.1107/S1600536809042196 |
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