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(3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate

The title compound, C(29)H(28)O(9), was isolated from the reaction of 4,6-dimeth­oxy-2-(4-methoxy­phen­yl)-3-benzofuran and α-methoxy­carbonyl­cinnaminate. The two aromatic rings form a dihedral angle of 22.7 (1)°. One methoxy­carbonyl group is disordered between two orientations in a 0.612 (4):0.38...

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Detalles Bibliográficos
Autores principales: Wang, Xian-You, Li, Nan, Ma, Yong-Qiang, Qin, Zhao-Hai
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971057/
https://www.ncbi.nlm.nih.gov/pubmed/21578476
http://dx.doi.org/10.1107/S1600536809042196
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author Wang, Xian-You
Li, Nan
Ma, Yong-Qiang
Qin, Zhao-Hai
author_facet Wang, Xian-You
Li, Nan
Ma, Yong-Qiang
Qin, Zhao-Hai
author_sort Wang, Xian-You
collection PubMed
description The title compound, C(29)H(28)O(9), was isolated from the reaction of 4,6-dimeth­oxy-2-(4-methoxy­phen­yl)-3-benzofuran and α-methoxy­carbonyl­cinnaminate. The two aromatic rings form a dihedral angle of 22.7 (1)°. One methoxy­carbonyl group is disordered between two orientations in a 0.612 (4):0.388 (4) ratio. The crystal structure exhibits no significantly short inter­molecular contacts.
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spelling pubmed-29710572010-12-30 (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate Wang, Xian-You Li, Nan Ma, Yong-Qiang Qin, Zhao-Hai Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(29)H(28)O(9), was isolated from the reaction of 4,6-dimeth­oxy-2-(4-methoxy­phen­yl)-3-benzofuran and α-methoxy­carbonyl­cinnaminate. The two aromatic rings form a dihedral angle of 22.7 (1)°. One methoxy­carbonyl group is disordered between two orientations in a 0.612 (4):0.388 (4) ratio. The crystal structure exhibits no significantly short inter­molecular contacts. International Union of Crystallography 2009-10-28 /pmc/articles/PMC2971057/ /pubmed/21578476 http://dx.doi.org/10.1107/S1600536809042196 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Xian-You
Li, Nan
Ma, Yong-Qiang
Qin, Zhao-Hai
(3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
title (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
title_full (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
title_fullStr (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
title_full_unstemmed (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
title_short (3R*)-Methyl 3-[(2S*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
title_sort (3r*)-methyl 3-[(2s*)-4,6-dimethoxy-2-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1-benzofuran-2-yl]-2-methoxycarbonyl-3-phenylpropionate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971057/
https://www.ncbi.nlm.nih.gov/pubmed/21578476
http://dx.doi.org/10.1107/S1600536809042196
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