10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide

In the title compound, C(13)H(15)NO(3)S, the sole classical hydrogen-bond donor is involved in an intra­molecular O—H⋯N hydrogen bond. In the crystal structure, pairs of mol­ecules related by inversion centres are linked by pairs of weak inter­molecular C—H⋯O inter­actions; these centrosymmetric pai...

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Detalles Bibliográficos
Autores principales: Patrick, B. O., Liang, H., Canesi, S., Ciufolini, M. A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971063/
https://www.ncbi.nlm.nih.gov/pubmed/21578237
http://dx.doi.org/10.1107/S1600536809038410
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author Patrick, B. O.
Liang, H.
Canesi, S.
Ciufolini, M. A.
author_facet Patrick, B. O.
Liang, H.
Canesi, S.
Ciufolini, M. A.
author_sort Patrick, B. O.
collection PubMed
description In the title compound, C(13)H(15)NO(3)S, the sole classical hydrogen-bond donor is involved in an intra­molecular O—H⋯N hydrogen bond. In the crystal structure, pairs of mol­ecules related by inversion centres are linked by pairs of weak inter­molecular C—H⋯O inter­actions; these centrosymmetric pairs are, in turn, linked further by weak inter­molecular C—H⋯O inter­actions, forming two-dimensional sheets oriented parallel to (101).
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spelling pubmed-29710632010-12-30 10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide Patrick, B. O. Liang, H. Canesi, S. Ciufolini, M. A. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(15)NO(3)S, the sole classical hydrogen-bond donor is involved in an intra­molecular O—H⋯N hydrogen bond. In the crystal structure, pairs of mol­ecules related by inversion centres are linked by pairs of weak inter­molecular C—H⋯O inter­actions; these centrosymmetric pairs are, in turn, linked further by weak inter­molecular C—H⋯O inter­actions, forming two-dimensional sheets oriented parallel to (101). International Union of Crystallography 2009-10-03 /pmc/articles/PMC2971063/ /pubmed/21578237 http://dx.doi.org/10.1107/S1600536809038410 Text en © Patrick et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Patrick, B. O.
Liang, H.
Canesi, S.
Ciufolini, M. A.
10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
title 10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
title_full 10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
title_fullStr 10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
title_full_unstemmed 10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
title_short 10-Ethynyl-2,3,6,6a,9,10-hexa­hydro-1H-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
title_sort 10-ethynyl-2,3,6,6a,9,10-hexa­hydro-1h-6,9-methano­pyrrolo[2,1-i][2,1]benzo­thia­zol-10-ol 5,5-dioxide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971063/
https://www.ncbi.nlm.nih.gov/pubmed/21578237
http://dx.doi.org/10.1107/S1600536809038410
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