N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide

In the title compound, C(16)H(8)Cl(2)F(2)N(4)O(2)S, the thia­diazole ring makes dihedral angles of 24.94 (14) and 48.11 (14)°, respectively, with the dichloro- and difluoro-substituted benzene rings. An intra­molecular N—H⋯O hydrogen bond results in the formation of a planar (mean deviation 0.0091 Å...

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Detalles Bibliográficos
Autores principales: Wang, Peng, Wan, Rong, Han, Feng, Wang, Yao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971195/
https://www.ncbi.nlm.nih.gov/pubmed/21578519
http://dx.doi.org/10.1107/S1600536809044584
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author Wang, Peng
Wan, Rong
Han, Feng
Wang, Yao
author_facet Wang, Peng
Wan, Rong
Han, Feng
Wang, Yao
author_sort Wang, Peng
collection PubMed
description In the title compound, C(16)H(8)Cl(2)F(2)N(4)O(2)S, the thia­diazole ring makes dihedral angles of 24.94 (14) and 48.11 (14)°, respectively, with the dichloro- and difluoro-substituted benzene rings. An intra­molecular N—H⋯O hydrogen bond results in the formation of a planar (mean deviation 0.0091 Å) six-membered ring. In the crystal structure, mol­ecules form centrosymmetric dimers through pairs of inter­molecular N—H⋯O hydrogen bonds.
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spelling pubmed-29711952010-12-30 N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide Wang, Peng Wan, Rong Han, Feng Wang, Yao Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(8)Cl(2)F(2)N(4)O(2)S, the thia­diazole ring makes dihedral angles of 24.94 (14) and 48.11 (14)°, respectively, with the dichloro- and difluoro-substituted benzene rings. An intra­molecular N—H⋯O hydrogen bond results in the formation of a planar (mean deviation 0.0091 Å) six-membered ring. In the crystal structure, mol­ecules form centrosymmetric dimers through pairs of inter­molecular N—H⋯O hydrogen bonds. International Union of Crystallography 2009-10-31 /pmc/articles/PMC2971195/ /pubmed/21578519 http://dx.doi.org/10.1107/S1600536809044584 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Peng
Wan, Rong
Han, Feng
Wang, Yao
N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
title N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
title_full N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
title_fullStr N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
title_full_unstemmed N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
title_short N-{N-[5-(2,4-Dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
title_sort n-{n-[5-(2,4-dichloro­phen­yl)-1,3,4-thia­diazol-2-yl]carbamo­yl}-2,6-difluoro­benzamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971195/
https://www.ncbi.nlm.nih.gov/pubmed/21578519
http://dx.doi.org/10.1107/S1600536809044584
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AT wanrong nn524dichlorophenyl134thiadiazol2ylcarbamoyl26difluorobenzamide
AT hanfeng nn524dichlorophenyl134thiadiazol2ylcarbamoyl26difluorobenzamide
AT wangyao nn524dichlorophenyl134thiadiazol2ylcarbamoyl26difluorobenzamide

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