Cargando…

1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate

In the title compound, C(16)H(13)N(5)O(3)S·CH(4)O, the dihedral angle between the isatin unit and the 2-methyl­phenyl group is 41.81 (2)° and intra­molecular N—H⋯O and N—H⋯N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N—H⋯...

Descripción completa

Detalles Bibliográficos
Autores principales: Pervez, Humayun, Yaqub, Muhammad, Manzoor, Nazia, Tahir, M. Nawaz, Iqbal, M. Saeed
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971320/
https://www.ncbi.nlm.nih.gov/pubmed/21578445
http://dx.doi.org/10.1107/S1600536809043633
_version_ 1782190599201357824
author Pervez, Humayun
Yaqub, Muhammad
Manzoor, Nazia
Tahir, M. Nawaz
Iqbal, M. Saeed
author_facet Pervez, Humayun
Yaqub, Muhammad
Manzoor, Nazia
Tahir, M. Nawaz
Iqbal, M. Saeed
author_sort Pervez, Humayun
collection PubMed
description In the title compound, C(16)H(13)N(5)O(3)S·CH(4)O, the dihedral angle between the isatin unit and the 2-methyl­phenyl group is 41.81 (2)° and intra­molecular N—H⋯O and N—H⋯N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N—H⋯O, O—H⋯S and C—H⋯O inter­actions.
format Text
id pubmed-2971320
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29713202010-12-30 1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate Pervez, Humayun Yaqub, Muhammad Manzoor, Nazia Tahir, M. Nawaz Iqbal, M. Saeed Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(13)N(5)O(3)S·CH(4)O, the dihedral angle between the isatin unit and the 2-methyl­phenyl group is 41.81 (2)° and intra­molecular N—H⋯O and N—H⋯N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N—H⋯O, O—H⋯S and C—H⋯O inter­actions. International Union of Crystallography 2009-10-28 /pmc/articles/PMC2971320/ /pubmed/21578445 http://dx.doi.org/10.1107/S1600536809043633 Text en © Pervez et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Pervez, Humayun
Yaqub, Muhammad
Manzoor, Nazia
Tahir, M. Nawaz
Iqbal, M. Saeed
1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
title 1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
title_full 1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
title_fullStr 1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
title_full_unstemmed 1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
title_short 1-(5-Nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
title_sort 1-(5-nitro-2-oxoindolin-3-yl­idene)-4-o-tolyl­thio­semicarbazide methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971320/
https://www.ncbi.nlm.nih.gov/pubmed/21578445
http://dx.doi.org/10.1107/S1600536809043633
work_keys_str_mv AT pervezhumayun 15nitro2oxoindolin3ylidene4otolylthiosemicarbazidemethanolmonosolvate
AT yaqubmuhammad 15nitro2oxoindolin3ylidene4otolylthiosemicarbazidemethanolmonosolvate
AT manzoornazia 15nitro2oxoindolin3ylidene4otolylthiosemicarbazidemethanolmonosolvate
AT tahirmnawaz 15nitro2oxoindolin3ylidene4otolylthiosemicarbazidemethanolmonosolvate
AT iqbalmsaeed 15nitro2oxoindolin3ylidene4otolylthiosemicarbazidemethanolmonosolvate