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1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate
In the title compound, C(16)H(13)N(5)O(3)S·CH(4)O, the dihedral angle between the isatin unit and the 2-methylphenyl group is 41.81 (2)° and intramolecular N—H⋯O and N—H⋯N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N—H⋯...
Autores principales: | , , , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971320/ https://www.ncbi.nlm.nih.gov/pubmed/21578445 http://dx.doi.org/10.1107/S1600536809043633 |
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author | Pervez, Humayun Yaqub, Muhammad Manzoor, Nazia Tahir, M. Nawaz Iqbal, M. Saeed |
author_facet | Pervez, Humayun Yaqub, Muhammad Manzoor, Nazia Tahir, M. Nawaz Iqbal, M. Saeed |
author_sort | Pervez, Humayun |
collection | PubMed |
description | In the title compound, C(16)H(13)N(5)O(3)S·CH(4)O, the dihedral angle between the isatin unit and the 2-methylphenyl group is 41.81 (2)° and intramolecular N—H⋯O and N—H⋯N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N—H⋯O, O—H⋯S and C—H⋯O interactions. |
format | Text |
id | pubmed-2971320 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29713202010-12-30 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate Pervez, Humayun Yaqub, Muhammad Manzoor, Nazia Tahir, M. Nawaz Iqbal, M. Saeed Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(13)N(5)O(3)S·CH(4)O, the dihedral angle between the isatin unit and the 2-methylphenyl group is 41.81 (2)° and intramolecular N—H⋯O and N—H⋯N hydrogen bonds occur, generating S(6) and S(5) rings, respectively. In the crystal, polymeric chains arise as a result of N—H⋯O, O—H⋯S and C—H⋯O interactions. International Union of Crystallography 2009-10-28 /pmc/articles/PMC2971320/ /pubmed/21578445 http://dx.doi.org/10.1107/S1600536809043633 Text en © Pervez et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Pervez, Humayun Yaqub, Muhammad Manzoor, Nazia Tahir, M. Nawaz Iqbal, M. Saeed 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
title | 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
title_full | 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
title_fullStr | 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
title_full_unstemmed | 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
title_short | 1-(5-Nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
title_sort | 1-(5-nitro-2-oxoindolin-3-ylidene)-4-o-tolylthiosemicarbazide methanol monosolvate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971320/ https://www.ncbi.nlm.nih.gov/pubmed/21578445 http://dx.doi.org/10.1107/S1600536809043633 |
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