1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)

The asymmetric unit of the title compound, C(12)H(14)N(4)·C(8)H(6)O(4)·4H(2)O, consists of one half of the 1,4-bis­(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) mol­ecule, one half of the terephthalic acid (TA) mol­ecule and two water mol­ecules. Both the bib and the TA mol­ecules reside on crystallog...

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Detalles Bibliográficos
Autores principales: Shang, Shao-Ming, Li, Su-Yun, Ren, Chun-Xia, Wang, Xin, Lu, Lu-De
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971323/
https://www.ncbi.nlm.nih.gov/pubmed/21578289
http://dx.doi.org/10.1107/S1600536809040616
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author Shang, Shao-Ming
Li, Su-Yun
Ren, Chun-Xia
Wang, Xin
Lu, Lu-De
author_facet Shang, Shao-Ming
Li, Su-Yun
Ren, Chun-Xia
Wang, Xin
Lu, Lu-De
author_sort Shang, Shao-Ming
collection PubMed
description The asymmetric unit of the title compound, C(12)H(14)N(4)·C(8)H(6)O(4)·4H(2)O, consists of one half of the 1,4-bis­(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) mol­ecule, one half of the terephthalic acid (TA) mol­ecule and two water mol­ecules. Both the bib and the TA mol­ecules reside on crystallographic inversion centers, which coincide with the centroids of the respective benzene rings. The bib and the TA, together with the water mol­ecules, are linked through inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds, forming a three-dimensional network of stacked layers. Weak inter­molecular C—H⋯O contacts support the stability of the crystal structure.
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spelling pubmed-29713232010-12-30 1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4) Shang, Shao-Ming Li, Su-Yun Ren, Chun-Xia Wang, Xin Lu, Lu-De Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(12)H(14)N(4)·C(8)H(6)O(4)·4H(2)O, consists of one half of the 1,4-bis­(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) mol­ecule, one half of the terephthalic acid (TA) mol­ecule and two water mol­ecules. Both the bib and the TA mol­ecules reside on crystallographic inversion centers, which coincide with the centroids of the respective benzene rings. The bib and the TA, together with the water mol­ecules, are linked through inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds, forming a three-dimensional network of stacked layers. Weak inter­molecular C—H⋯O contacts support the stability of the crystal structure. International Union of Crystallography 2009-10-10 /pmc/articles/PMC2971323/ /pubmed/21578289 http://dx.doi.org/10.1107/S1600536809040616 Text en © Shang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shang, Shao-Ming
Li, Su-Yun
Ren, Chun-Xia
Wang, Xin
Lu, Lu-De
1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
title 1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
title_full 1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
title_fullStr 1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
title_full_unstemmed 1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
title_short 1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
title_sort 1,4-bis(4,5-dihydro-1h-imidazol-2-yl)benzene–terephthalic acid–water (1/1/4)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971323/
https://www.ncbi.nlm.nih.gov/pubmed/21578289
http://dx.doi.org/10.1107/S1600536809040616
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