3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate

In the title compound, C(13)H(13)FN(4)O(3)·0.5CH(3)OH, mol­ecules are packed in the crystal structure by a series of O—H⋯N, N—H⋯O, N—H⋯F and O—H⋯O inter­molecular hydrogen bonds. The indole and creatinine units make a dihedral angle of 60.80 (4)°.

Detalles Bibliográficos
Autores principales: Penthala, Narsimha Reddy, Reddy, Thirupathi Reddy Yerram, Parkin, Sean, Crooks, Peter A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971372/
https://www.ncbi.nlm.nih.gov/pubmed/21578489
http://dx.doi.org/10.1107/S1600536809043797
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author Penthala, Narsimha Reddy
Reddy, Thirupathi Reddy Yerram
Parkin, Sean
Crooks, Peter A.
author_facet Penthala, Narsimha Reddy
Reddy, Thirupathi Reddy Yerram
Parkin, Sean
Crooks, Peter A.
author_sort Penthala, Narsimha Reddy
collection PubMed
description In the title compound, C(13)H(13)FN(4)O(3)·0.5CH(3)OH, mol­ecules are packed in the crystal structure by a series of O—H⋯N, N—H⋯O, N—H⋯F and O—H⋯O inter­molecular hydrogen bonds. The indole and creatinine units make a dihedral angle of 60.80 (4)°.
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spelling pubmed-29713722010-12-30 3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate Penthala, Narsimha Reddy Reddy, Thirupathi Reddy Yerram Parkin, Sean Crooks, Peter A. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(13)FN(4)O(3)·0.5CH(3)OH, mol­ecules are packed in the crystal structure by a series of O—H⋯N, N—H⋯O, N—H⋯F and O—H⋯O inter­molecular hydrogen bonds. The indole and creatinine units make a dihedral angle of 60.80 (4)°. International Union of Crystallography 2009-10-31 /pmc/articles/PMC2971372/ /pubmed/21578489 http://dx.doi.org/10.1107/S1600536809043797 Text en © Penthala et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Penthala, Narsimha Reddy
Reddy, Thirupathi Reddy Yerram
Parkin, Sean
Crooks, Peter A.
3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
title 3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
title_full 3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
title_fullStr 3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
title_full_unstemmed 3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
title_short 3-(2-Amino-1-methyl-4-oxo-4,5-dihydro-1H-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
title_sort 3-(2-amino-1-methyl-4-oxo-4,5-dihydro-1h-imidazol-5-yl)-5-fluoro-3-hydr­oxy-1-methyl­indolin-2-one methanol hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971372/
https://www.ncbi.nlm.nih.gov/pubmed/21578489
http://dx.doi.org/10.1107/S1600536809043797
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AT reddythirupathireddyyerram 32amino1methyl4oxo45dihydro1himidazol5yl5fluoro3hydroxy1methylindolin2onemethanolhemisolvate
AT parkinsean 32amino1methyl4oxo45dihydro1himidazol5yl5fluoro3hydroxy1methylindolin2onemethanolhemisolvate
AT crookspetera 32amino1methyl4oxo45dihydro1himidazol5yl5fluoro3hydroxy1methylindolin2onemethanolhemisolvate

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