3-Bromo­anilinium picrate

In the title compound, C(6)H(7)BrN(+)·C(6)H(2)N(3)O(7) (−), the O atoms of two of the nitro groups are disordered over two sites, the ratios of the refined occupancies being 0.72 (6):0.28 (6) and 0.74 (5):0.26 (5). In the crystal structure, the anions and cations are linked via inter­molecular N—H⋯O...

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Detalles Bibliográficos
Autores principales: Li, Yan-jun, Zhao, Bo
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971793/
https://www.ncbi.nlm.nih.gov/pubmed/21578926
http://dx.doi.org/10.1107/S1600536809048405
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author Li, Yan-jun
Zhao, Bo
author_facet Li, Yan-jun
Zhao, Bo
author_sort Li, Yan-jun
collection PubMed
description In the title compound, C(6)H(7)BrN(+)·C(6)H(2)N(3)O(7) (−), the O atoms of two of the nitro groups are disordered over two sites, the ratios of the refined occupancies being 0.72 (6):0.28 (6) and 0.74 (5):0.26 (5). In the crystal structure, the anions and cations are linked via inter­molecular N—H⋯O hydrogen bonds into chains along [100]. Further stabilization is provided by weak inter­molecular C—H⋯O hydrogen bonds.
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spelling pubmed-29717932010-12-30 3-Bromo­anilinium picrate Li, Yan-jun Zhao, Bo Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(6)H(7)BrN(+)·C(6)H(2)N(3)O(7) (−), the O atoms of two of the nitro groups are disordered over two sites, the ratios of the refined occupancies being 0.72 (6):0.28 (6) and 0.74 (5):0.26 (5). In the crystal structure, the anions and cations are linked via inter­molecular N—H⋯O hydrogen bonds into chains along [100]. Further stabilization is provided by weak inter­molecular C—H⋯O hydrogen bonds. International Union of Crystallography 2009-11-25 /pmc/articles/PMC2971793/ /pubmed/21578926 http://dx.doi.org/10.1107/S1600536809048405 Text en © Li and Zhao 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Yan-jun
Zhao, Bo
3-Bromo­anilinium picrate
title 3-Bromo­anilinium picrate
title_full 3-Bromo­anilinium picrate
title_fullStr 3-Bromo­anilinium picrate
title_full_unstemmed 3-Bromo­anilinium picrate
title_short 3-Bromo­anilinium picrate
title_sort 3-bromo­anilinium picrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971793/
https://www.ncbi.nlm.nih.gov/pubmed/21578926
http://dx.doi.org/10.1107/S1600536809048405
work_keys_str_mv AT liyanjun 3bromoaniliniumpicrate
AT zhaobo 3bromoaniliniumpicrate

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