(E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene

The title compound, C(18)H(18)Cl(2)N(2)O(2), was synthesized by the reaction of 1-(5-chloro-2-methoxy­phen­yl)ethanone with hydrazine hydrate. The mol­ecule lies on a crystallographic twofold axis passing through the mid-point of the N—N bond with one half-mol­ecule in the asymmetric unit. The dihed...

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Detalles Bibliográficos
Autores principales: Chang, Jian-Guo, Lu, Jie, Zhao, Ren-Gao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971795/
https://www.ncbi.nlm.nih.gov/pubmed/21578897
http://dx.doi.org/10.1107/S1600536809048351
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author Chang, Jian-Guo
Lu, Jie
Zhao, Ren-Gao
author_facet Chang, Jian-Guo
Lu, Jie
Zhao, Ren-Gao
author_sort Chang, Jian-Guo
collection PubMed
description The title compound, C(18)H(18)Cl(2)N(2)O(2), was synthesized by the reaction of 1-(5-chloro-2-methoxy­phen­yl)ethanone with hydrazine hydrate. The mol­ecule lies on a crystallographic twofold axis passing through the mid-point of the N—N bond with one half-mol­ecule in the asymmetric unit. The dihedral angle between the two aromatic rings is 44.33 (4)°. In the crystal, inter­molecular C—H⋯O inter­actions link the mol­ecules into columns along the c axis
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spelling pubmed-29717952010-12-30 (E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene Chang, Jian-Guo Lu, Jie Zhao, Ren-Gao Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(18)H(18)Cl(2)N(2)O(2), was synthesized by the reaction of 1-(5-chloro-2-methoxy­phen­yl)ethanone with hydrazine hydrate. The mol­ecule lies on a crystallographic twofold axis passing through the mid-point of the N—N bond with one half-mol­ecule in the asymmetric unit. The dihedral angle between the two aromatic rings is 44.33 (4)°. In the crystal, inter­molecular C—H⋯O inter­actions link the mol­ecules into columns along the c axis International Union of Crystallography 2009-11-25 /pmc/articles/PMC2971795/ /pubmed/21578897 http://dx.doi.org/10.1107/S1600536809048351 Text en © Chang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chang, Jian-Guo
Lu, Jie
Zhao, Ren-Gao
(E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
title (E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
title_full (E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
title_fullStr (E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
title_full_unstemmed (E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
title_short (E,E)-2,5-Bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
title_sort (e,e)-2,5-bis(5-chloro-2-methoxyphenyl)-3,4-diazahexa-2,4-diene
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971795/
https://www.ncbi.nlm.nih.gov/pubmed/21578897
http://dx.doi.org/10.1107/S1600536809048351
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