3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate

The title monohydrate, C(17)H(11)ClN(4)·H(2)O, features an essentially planar organic mol­ecule, as seen in the dihedral angle of 2.42 (8)° formed between the quinoline and benzene planes. The conformation about the imine bond is E, and the N—H group is oriented towards the quinoline residue. The ma...

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Detalles Bibliográficos
Autores principales: de Ferreira, Marcelle L., de Souza, Marcus V. N., Howie, R. Alan, Tiekink, Edward R. T., Wardell, James L., Wardell, Solange M. S. V.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971809/
https://www.ncbi.nlm.nih.gov/pubmed/21578942
http://dx.doi.org/10.1107/S1600536809050120
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author de Ferreira, Marcelle L.
de Souza, Marcus V. N.
Howie, R. Alan
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
author_facet de Ferreira, Marcelle L.
de Souza, Marcus V. N.
Howie, R. Alan
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
author_sort de Ferreira, Marcelle L.
collection PubMed
description The title monohydrate, C(17)H(11)ClN(4)·H(2)O, features an essentially planar organic mol­ecule, as seen in the dihedral angle of 2.42 (8)° formed between the quinoline and benzene planes. The conformation about the imine bond is E, and the N—H group is oriented towards the quinoline residue. The major feature of the crystal packing is the formation of supra­molecular chains along [100], whereby the water mol­ecule accepts one N—H⋯O hydrogen bond and makes two O—H⋯N hydrogen bonds. A C—H⋯O link is also present.
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spelling pubmed-29718092010-12-30 3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate de Ferreira, Marcelle L. de Souza, Marcus V. N. Howie, R. Alan Tiekink, Edward R. T. Wardell, James L. Wardell, Solange M. S. V. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title monohydrate, C(17)H(11)ClN(4)·H(2)O, features an essentially planar organic mol­ecule, as seen in the dihedral angle of 2.42 (8)° formed between the quinoline and benzene planes. The conformation about the imine bond is E, and the N—H group is oriented towards the quinoline residue. The major feature of the crystal packing is the formation of supra­molecular chains along [100], whereby the water mol­ecule accepts one N—H⋯O hydrogen bond and makes two O—H⋯N hydrogen bonds. A C—H⋯O link is also present. International Union of Crystallography 2009-11-28 /pmc/articles/PMC2971809/ /pubmed/21578942 http://dx.doi.org/10.1107/S1600536809050120 Text en © Ferreira et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
de Ferreira, Marcelle L.
de Souza, Marcus V. N.
Howie, R. Alan
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
title 3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
title_full 3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
title_fullStr 3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
title_full_unstemmed 3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
title_short 3-[(E)-(7-Chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
title_sort 3-[(e)-(7-chloro-4-quinol­yl)hydrazono­meth­yl]benzonitrile monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971809/
https://www.ncbi.nlm.nih.gov/pubmed/21578942
http://dx.doi.org/10.1107/S1600536809050120
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