2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate

The title hydrate, C(10)H(10)N(4)·H(2)O, shows a small twist in the hydro­zone derivative, the dihedral angle between the pyridine and pyrrole rings being 11.08 (12)°. The pyridine and pyrrole N atoms lie to the same side of the mol­ecule being sustained in place by hydrogen-bonding inter­actions wi...

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Detalles Bibliográficos
Autores principales: de Lima, Geraldo M., Tiekink, Edward R. T., Wardell, James L., Wardell, Solange M. S. V.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971851/
https://www.ncbi.nlm.nih.gov/pubmed/21578943
http://dx.doi.org/10.1107/S1600536809050296
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author de Lima, Geraldo M.
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
author_facet de Lima, Geraldo M.
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
author_sort de Lima, Geraldo M.
collection PubMed
description The title hydrate, C(10)H(10)N(4)·H(2)O, shows a small twist in the hydro­zone derivative, the dihedral angle between the pyridine and pyrrole rings being 11.08 (12)°. The pyridine and pyrrole N atoms lie to the same side of the mol­ecule being sustained in place by hydrogen-bonding inter­actions with the water mol­ecule. Further inter­molecular O—H⋯N and N—H⋯O hydrogen bonding leads to the formation of supra­molecular arrays in the ab plane.
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spelling pubmed-29718512010-12-30 2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate de Lima, Geraldo M. Tiekink, Edward R. T. Wardell, James L. Wardell, Solange M. S. V. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title hydrate, C(10)H(10)N(4)·H(2)O, shows a small twist in the hydro­zone derivative, the dihedral angle between the pyridine and pyrrole rings being 11.08 (12)°. The pyridine and pyrrole N atoms lie to the same side of the mol­ecule being sustained in place by hydrogen-bonding inter­actions with the water mol­ecule. Further inter­molecular O—H⋯N and N—H⋯O hydrogen bonding leads to the formation of supra­molecular arrays in the ab plane. International Union of Crystallography 2009-11-28 /pmc/articles/PMC2971851/ /pubmed/21578943 http://dx.doi.org/10.1107/S1600536809050296 Text en © Lima et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
de Lima, Geraldo M.
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
title 2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
title_full 2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
title_fullStr 2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
title_full_unstemmed 2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
title_short 2-[(E)-(1H-Pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
title_sort 2-[(e)-(1h-pyrrol-2-ylmethyl­idene)hydrazinyl]pyridine monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971851/
https://www.ncbi.nlm.nih.gov/pubmed/21578943
http://dx.doi.org/10.1107/S1600536809050296
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