Bis(4-hydroxy­pyridinium) sulfate monohydrate

In the crystal structure of the title salt, 2C(5)H(6)NO(+)·SO(4) (2−)·H(2)O, one planar (r.m.s. deviation = 0.01 Å) cation is stacked approximately over the other [dihedral angle between planes = 8.6 (1)°]. The pyridinium and hydr­oxy H atoms are hydrogen-bond donor atoms to the O atoms of the sulfa...

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Detalles Bibliográficos
Autores principales: Xu, Ying-Ming, Gao, Shan, Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971874/
https://www.ncbi.nlm.nih.gov/pubmed/21578865
http://dx.doi.org/10.1107/S1600536809048521
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author Xu, Ying-Ming
Gao, Shan
Ng, Seik Weng
author_facet Xu, Ying-Ming
Gao, Shan
Ng, Seik Weng
author_sort Xu, Ying-Ming
collection PubMed
description In the crystal structure of the title salt, 2C(5)H(6)NO(+)·SO(4) (2−)·H(2)O, one planar (r.m.s. deviation = 0.01 Å) cation is stacked approximately over the other [dihedral angle between planes = 8.6 (1)°]. The pyridinium and hydr­oxy H atoms are hydrogen-bond donor atoms to the O atoms of the sulfate anion; the cations, anions and water mol­ecules are consolidated into a three-dimensional network through O—H⋯O and N—H⋯O hydrogen bonds.
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spelling pubmed-29718742010-12-30 Bis(4-hydroxy­pyridinium) sulfate monohydrate Xu, Ying-Ming Gao, Shan Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title salt, 2C(5)H(6)NO(+)·SO(4) (2−)·H(2)O, one planar (r.m.s. deviation = 0.01 Å) cation is stacked approximately over the other [dihedral angle between planes = 8.6 (1)°]. The pyridinium and hydr­oxy H atoms are hydrogen-bond donor atoms to the O atoms of the sulfate anion; the cations, anions and water mol­ecules are consolidated into a three-dimensional network through O—H⋯O and N—H⋯O hydrogen bonds. International Union of Crystallography 2009-11-21 /pmc/articles/PMC2971874/ /pubmed/21578865 http://dx.doi.org/10.1107/S1600536809048521 Text en © Xu et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xu, Ying-Ming
Gao, Shan
Ng, Seik Weng
Bis(4-hydroxy­pyridinium) sulfate monohydrate
title Bis(4-hydroxy­pyridinium) sulfate monohydrate
title_full Bis(4-hydroxy­pyridinium) sulfate monohydrate
title_fullStr Bis(4-hydroxy­pyridinium) sulfate monohydrate
title_full_unstemmed Bis(4-hydroxy­pyridinium) sulfate monohydrate
title_short Bis(4-hydroxy­pyridinium) sulfate monohydrate
title_sort bis(4-hydroxy­pyridinium) sulfate monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971874/
https://www.ncbi.nlm.nih.gov/pubmed/21578865
http://dx.doi.org/10.1107/S1600536809048521
work_keys_str_mv AT xuyingming bis4hydroxypyridiniumsulfatemonohydrate
AT gaoshan bis4hydroxypyridiniumsulfatemonohydrate
AT ngseikweng bis4hydroxypyridiniumsulfatemonohydrate

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