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N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate
In the structure of the title compound, C(12)H(11)N(3)O(3)·H(2)O, the dihedral angle formed by the benzene and isoxazole rings is 2.03 (8)°. The molecular conformation is stabilized by an intramolecular O—H⋯N hydrogen bond. In the crystal structure, molecules are linked into a three-dimesional ne...
Autores principales: | , , , , |
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971927/ https://www.ncbi.nlm.nih.gov/pubmed/21578839 http://dx.doi.org/10.1107/S1600536809048028 |
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author | Jin, Yan-Xian Yan, Zhen-Zhong Yang, Jian-Guo Zhong, Ai-Guo Pan, Fu-You |
author_facet | Jin, Yan-Xian Yan, Zhen-Zhong Yang, Jian-Guo Zhong, Ai-Guo Pan, Fu-You |
author_sort | Jin, Yan-Xian |
collection | PubMed |
description | In the structure of the title compound, C(12)H(11)N(3)O(3)·H(2)O, the dihedral angle formed by the benzene and isoxazole rings is 2.03 (8)°. The molecular conformation is stabilized by an intramolecular O—H⋯N hydrogen bond. In the crystal structure, molecules are linked into a three-dimesional network by intermolecular N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, and by π–π stacking interactions involving adjacent benzene and isoxazole rings [centroid–centroid separation = 3.663 (2) Å]. |
format | Text |
id | pubmed-2971927 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29719272010-12-30 N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate Jin, Yan-Xian Yan, Zhen-Zhong Yang, Jian-Guo Zhong, Ai-Guo Pan, Fu-You Acta Crystallogr Sect E Struct Rep Online Organic Papers In the structure of the title compound, C(12)H(11)N(3)O(3)·H(2)O, the dihedral angle formed by the benzene and isoxazole rings is 2.03 (8)°. The molecular conformation is stabilized by an intramolecular O—H⋯N hydrogen bond. In the crystal structure, molecules are linked into a three-dimesional network by intermolecular N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, and by π–π stacking interactions involving adjacent benzene and isoxazole rings [centroid–centroid separation = 3.663 (2) Å]. International Union of Crystallography 2009-11-18 /pmc/articles/PMC2971927/ /pubmed/21578839 http://dx.doi.org/10.1107/S1600536809048028 Text en © Jin et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Jin, Yan-Xian Yan, Zhen-Zhong Yang, Jian-Guo Zhong, Ai-Guo Pan, Fu-You N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
title |
N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
title_full |
N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
title_fullStr |
N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
title_full_unstemmed |
N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
title_short |
N′-[(E)-2-Hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
title_sort | n′-[(e)-2-hydroxybenzylidene]-5-methylisoxazole-4-carbohydrazide monohydrate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971927/ https://www.ncbi.nlm.nih.gov/pubmed/21578839 http://dx.doi.org/10.1107/S1600536809048028 |
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