3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate

In the title spiro­diclofen derivative, C(22)H(17)Cl(3)O(4), the cyclo­hexane ring adopts a chair conformation [four C atoms are planar with a mean deviation of 0.018 Å and the two C atoms at the flap positions deviate by 0.613 (4) and −0.668 (5) Å from the plane]. The dihedral angles between the fu...

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Detalles Bibliográficos
Autores principales: Zhou, Yong, Cheng, Jing-Li, Zhu, Guo-Nian, Zhao, Jin-Hao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971930/
https://www.ncbi.nlm.nih.gov/pubmed/21578732
http://dx.doi.org/10.1107/S1600536809044109
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author Zhou, Yong
Cheng, Jing-Li
Zhu, Guo-Nian
Zhao, Jin-Hao
author_facet Zhou, Yong
Cheng, Jing-Li
Zhu, Guo-Nian
Zhao, Jin-Hao
author_sort Zhou, Yong
collection PubMed
description In the title spiro­diclofen derivative, C(22)H(17)Cl(3)O(4), the cyclo­hexane ring adopts a chair conformation [four C atoms are planar with a mean deviation of 0.018 Å and the two C atoms at the flap positions deviate by 0.613 (4) and −0.668 (5) Å from the plane]. The dihedral angles between the furan ring and the two benzene rings are 55.78 (3) and 49.92 (3)°. Weak inter­molecular C—H⋯Cl inter­actions are observed in the crystal structure.
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spelling pubmed-29719302010-12-30 3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate Zhou, Yong Cheng, Jing-Li Zhu, Guo-Nian Zhao, Jin-Hao Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title spiro­diclofen derivative, C(22)H(17)Cl(3)O(4), the cyclo­hexane ring adopts a chair conformation [four C atoms are planar with a mean deviation of 0.018 Å and the two C atoms at the flap positions deviate by 0.613 (4) and −0.668 (5) Å from the plane]. The dihedral angles between the furan ring and the two benzene rings are 55.78 (3) and 49.92 (3)°. Weak inter­molecular C—H⋯Cl inter­actions are observed in the crystal structure. International Union of Crystallography 2009-11-04 /pmc/articles/PMC2971930/ /pubmed/21578732 http://dx.doi.org/10.1107/S1600536809044109 Text en © Zhou et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhou, Yong
Cheng, Jing-Li
Zhu, Guo-Nian
Zhao, Jin-Hao
3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
title 3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
title_full 3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
title_fullStr 3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
title_full_unstemmed 3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
title_short 3-(2,4-Dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
title_sort 3-(2,4-dichloro­phen­yl)-2-oxo-1-oxa­spiro­[4.5]dec-3-en-4-yl 4-chloro­benzoate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971930/
https://www.ncbi.nlm.nih.gov/pubmed/21578732
http://dx.doi.org/10.1107/S1600536809044109
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