2-Methyl-2,4-di-4-pyridyl-2,3-dihydro-1H-1,5-benzodiazepine acetic acid solvate

In the title compound, C(20)H(18)N(4)·CH(3)COOH, the benzene ring forms dihedral angles of 81.34 (11) and 54.32 (11)° with the two pyridine rings. In the crystal, inter­molecular O—H⋯N hydrogen bonding links one 1,5-benzodiazepine mol­ecule and one acetic acid solvent mol­ecule into a dimer. These d...

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Detalles Bibliográficos
Autores principales: Wang, Shi-Chao, Hou, Qiu-Fei, Jiang, Shi-Mei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2971997/
https://www.ncbi.nlm.nih.gov/pubmed/21578921
http://dx.doi.org/10.1107/S1600536809049836
Descripción
Sumario:In the title compound, C(20)H(18)N(4)·CH(3)COOH, the benzene ring forms dihedral angles of 81.34 (11) and 54.32 (11)° with the two pyridine rings. In the crystal, inter­molecular O—H⋯N hydrogen bonding links one 1,5-benzodiazepine mol­ecule and one acetic acid solvent mol­ecule into a dimer. These dimers, related by translation along the b axis, are further linked into chains via weak inter­molecular N—H⋯N hydrogen bonds.

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