Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate

In the crystal structure of the title salt, 3C(5)H(6)NO(+)·HSO(4) (−)·SO(4) (2−)·H(2)O, the hydrogen sulfate ion is linked to the sulfate ion by an O—H⋯O hydrogen bond. The hydrogen sulfate–sulfate anion is a hydrogen-bond acceptor for the three independent cations and the uncoordinated water mol­ec...

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Detalles Bibliográficos
Autores principales: Xu, Ying-Ming, Gao, Shan, Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2972122/
https://www.ncbi.nlm.nih.gov/pubmed/21578866
http://dx.doi.org/10.1107/S1600536809048545
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author Xu, Ying-Ming
Gao, Shan
Ng, Seik Weng
author_facet Xu, Ying-Ming
Gao, Shan
Ng, Seik Weng
author_sort Xu, Ying-Ming
collection PubMed
description In the crystal structure of the title salt, 3C(5)H(6)NO(+)·HSO(4) (−)·SO(4) (2−)·H(2)O, the hydrogen sulfate ion is linked to the sulfate ion by an O—H⋯O hydrogen bond. The hydrogen sulfate–sulfate anion is a hydrogen-bond acceptor for the three independent cations and the uncoordinated water mol­ecule, the hydrogen-bonding inter­actions giving rise to a three-dimensional hydrogen-bonded network. In the hydrogen sulfate–sulfate species, one of the sulfate groups is disordered in respect of its O atoms in a 2:1 ratio.
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spelling pubmed-29721222010-12-30 Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate Xu, Ying-Ming Gao, Shan Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title salt, 3C(5)H(6)NO(+)·HSO(4) (−)·SO(4) (2−)·H(2)O, the hydrogen sulfate ion is linked to the sulfate ion by an O—H⋯O hydrogen bond. The hydrogen sulfate–sulfate anion is a hydrogen-bond acceptor for the three independent cations and the uncoordinated water mol­ecule, the hydrogen-bonding inter­actions giving rise to a three-dimensional hydrogen-bonded network. In the hydrogen sulfate–sulfate species, one of the sulfate groups is disordered in respect of its O atoms in a 2:1 ratio. International Union of Crystallography 2009-11-21 /pmc/articles/PMC2972122/ /pubmed/21578866 http://dx.doi.org/10.1107/S1600536809048545 Text en © Xu et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xu, Ying-Ming
Gao, Shan
Ng, Seik Weng
Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
title Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
title_full Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
title_fullStr Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
title_full_unstemmed Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
title_short Tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
title_sort tris(4-hydroxy­pyridinium) hydrogen sulfate–sulfate monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2972122/
https://www.ncbi.nlm.nih.gov/pubmed/21578866
http://dx.doi.org/10.1107/S1600536809048545
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AT gaoshan tris4hydroxypyridiniumhydrogensulfatesulfatemonohydrate
AT ngseikweng tris4hydroxypyridiniumhydrogensulfatesulfatemonohydrate

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