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(E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)

In the title compound, C(20)H(19)N(3)O(4)·CH(4)O·H(2)O, the Schiff base mol­ecule is almost planar, with a dihedral angle of 1.2 (1)° between the benzene ring and the quinoline ring system. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring. In the crystal, the methanol and water solvent...

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Detalles Bibliográficos
Autor principal: Ma, Zhan-Ling
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2972133/
https://www.ncbi.nlm.nih.gov/pubmed/21578936
http://dx.doi.org/10.1107/S1600536809051034
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author Ma, Zhan-Ling
author_facet Ma, Zhan-Ling
author_sort Ma, Zhan-Ling
collection PubMed
description In the title compound, C(20)H(19)N(3)O(4)·CH(4)O·H(2)O, the Schiff base mol­ecule is almost planar, with a dihedral angle of 1.2 (1)° between the benzene ring and the quinoline ring system. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring. In the crystal, the methanol and water solvent mol­ecules are linked to the Schiff base mol­ecule via N—H⋯O, O—H⋯O, O—H⋯N and O—H⋯(O,N) hydrogen bonds.
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spelling pubmed-29721332010-12-30 (E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1) Ma, Zhan-Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(20)H(19)N(3)O(4)·CH(4)O·H(2)O, the Schiff base mol­ecule is almost planar, with a dihedral angle of 1.2 (1)° between the benzene ring and the quinoline ring system. An intra­molecular N—H⋯O hydrogen bond generates an S(6) ring. In the crystal, the methanol and water solvent mol­ecules are linked to the Schiff base mol­ecule via N—H⋯O, O—H⋯O, O—H⋯N and O—H⋯(O,N) hydrogen bonds. International Union of Crystallography 2009-11-28 /pmc/articles/PMC2972133/ /pubmed/21578936 http://dx.doi.org/10.1107/S1600536809051034 Text en © Zhan-Ling Ma 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ma, Zhan-Ling
(E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
title (E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
title_full (E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
title_fullStr (E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
title_full_unstemmed (E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
title_short (E)-N′-(3,4-Dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
title_sort (e)-n′-(3,4-dimethoxy­benzyl­idene)-2-(8-quinol­yloxy)acetohydrazide–methanol–water (1/1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2972133/
https://www.ncbi.nlm.nih.gov/pubmed/21578936
http://dx.doi.org/10.1107/S1600536809051034
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