3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate

The asymmetric unit of the title compound, C(14)H(11)NO(2)·0.33H(2)O, contains three 3-hydr­oxy-3-phenyl­isoindolin-1-one (HPIO) mol­ecules and one water mol­ecule. The three independent HPIO mol­ecules differ in the orientations of hydr­oxy and phenyl groups substituted at the 3-position with respe...

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Detalles Bibliográficos
Autores principales: Liu, Shan, Zhang, Xiao-Li, Zhang, Wen-Hong, Zhu, Hong-Jun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2972140/
https://www.ncbi.nlm.nih.gov/pubmed/21578748
http://dx.doi.org/10.1107/S160053680904608X
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author Liu, Shan
Zhang, Xiao-Li
Zhang, Wen-Hong
Zhu, Hong-Jun
author_facet Liu, Shan
Zhang, Xiao-Li
Zhang, Wen-Hong
Zhu, Hong-Jun
author_sort Liu, Shan
collection PubMed
description The asymmetric unit of the title compound, C(14)H(11)NO(2)·0.33H(2)O, contains three 3-hydr­oxy-3-phenyl­isoindolin-1-one (HPIO) mol­ecules and one water mol­ecule. The three independent HPIO mol­ecules differ in the orientations of hydr­oxy and phenyl groups substituted at the 3-position with respect to the planar [r.m.s. deviations of 0.0173, 0.0170 and 0.0102 Å] dihydro­isoindolin-1-one ring system. In the crystal structure, mol­ecules are linked into a three-dimensional network by O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds.
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spelling pubmed-29721402010-12-30 3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate Liu, Shan Zhang, Xiao-Li Zhang, Wen-Hong Zhu, Hong-Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(11)NO(2)·0.33H(2)O, contains three 3-hydr­oxy-3-phenyl­isoindolin-1-one (HPIO) mol­ecules and one water mol­ecule. The three independent HPIO mol­ecules differ in the orientations of hydr­oxy and phenyl groups substituted at the 3-position with respect to the planar [r.m.s. deviations of 0.0173, 0.0170 and 0.0102 Å] dihydro­isoindolin-1-one ring system. In the crystal structure, mol­ecules are linked into a three-dimensional network by O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds. International Union of Crystallography 2009-11-07 /pmc/articles/PMC2972140/ /pubmed/21578748 http://dx.doi.org/10.1107/S160053680904608X Text en © Liu et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liu, Shan
Zhang, Xiao-Li
Zhang, Wen-Hong
Zhu, Hong-Jun
3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
title 3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
title_full 3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
title_fullStr 3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
title_full_unstemmed 3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
title_short 3-Hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
title_sort 3-hydr­oxy-3-phenyl­isoindolin-1-one 0.33-hydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2972140/
https://www.ncbi.nlm.nih.gov/pubmed/21578748
http://dx.doi.org/10.1107/S160053680904608X
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AT zhangxiaoli 3hydroxy3phenylisoindolin1one033hydrate
AT zhangwenhong 3hydroxy3phenylisoindolin1one033hydrate
AT zhuhongjun 3hydroxy3phenylisoindolin1one033hydrate

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