4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione

In the title mol­ecule, C(11)H(16)O(2)S(5), the two S atoms from the macrocycle are situated on opposite sides of the mean plane of the five-membered ring, deviating from it by 1.288 (3) and 1.728 (3) Å. In the crystal, weak inter­molecular C—H⋯S and C—H⋯O hydrogen bonds link the mol­ecules into lay...

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Detalles Bibliográficos
Autores principales: Hou, Rui-Bin, Li, Bao, Chen, Tie, Yin, Bing-Zhu, Wu, Li-Xin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977179/
https://www.ncbi.nlm.nih.gov/pubmed/21583706
http://dx.doi.org/10.1107/S1600536809029468
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author Hou, Rui-Bin
Li, Bao
Chen, Tie
Yin, Bing-Zhu
Wu, Li-Xin
author_facet Hou, Rui-Bin
Li, Bao
Chen, Tie
Yin, Bing-Zhu
Wu, Li-Xin
author_sort Hou, Rui-Bin
collection PubMed
description In the title mol­ecule, C(11)H(16)O(2)S(5), the two S atoms from the macrocycle are situated on opposite sides of the mean plane of the five-membered ring, deviating from it by 1.288 (3) and 1.728 (3) Å. In the crystal, weak inter­molecular C—H⋯S and C—H⋯O hydrogen bonds link the mol­ecules into layers parallel to (100). The crystal studied was a racemic twin.
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spelling pubmed-29771792010-12-30 4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione Hou, Rui-Bin Li, Bao Chen, Tie Yin, Bing-Zhu Wu, Li-Xin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(11)H(16)O(2)S(5), the two S atoms from the macrocycle are situated on opposite sides of the mean plane of the five-membered ring, deviating from it by 1.288 (3) and 1.728 (3) Å. In the crystal, weak inter­molecular C—H⋯S and C—H⋯O hydrogen bonds link the mol­ecules into layers parallel to (100). The crystal studied was a racemic twin. International Union of Crystallography 2009-07-31 /pmc/articles/PMC2977179/ /pubmed/21583706 http://dx.doi.org/10.1107/S1600536809029468 Text en © Hou et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hou, Rui-Bin
Li, Bao
Chen, Tie
Yin, Bing-Zhu
Wu, Li-Xin
4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
title 4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
title_full 4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
title_fullStr 4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
title_full_unstemmed 4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
title_short 4,6,7,9,10,12,13,15-Octa­hydro-2H-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
title_sort 4,6,7,9,10,12,13,15-octa­hydro-2h-1,3-dithiolo[4,5-i][1,4,7,12]dioxadithia­cyclo­tetra­decine-2-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977179/
https://www.ncbi.nlm.nih.gov/pubmed/21583706
http://dx.doi.org/10.1107/S1600536809029468
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