3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one

The title compound, C(13)H(15)NO(3), was synthesized by the Aldol reaction of isatin and 3-methyl­butan-2-one refluxing in methanol catalyzed by dimethyl­amine. The packing of the mol­ecules in the crystal structure features inter­molecular N—H⋯O and O—H⋯O hydrogen bonds.

Detalles Bibliográficos
Autores principales: Chen, Gang, Liu, Bin, Tang, Ying, Xu, Jingfang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977200/
https://www.ncbi.nlm.nih.gov/pubmed/21583440
http://dx.doi.org/10.1107/S1600536809024611
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author Chen, Gang
Liu, Bin
Tang, Ying
Xu, Jingfang
author_facet Chen, Gang
Liu, Bin
Tang, Ying
Xu, Jingfang
author_sort Chen, Gang
collection PubMed
description The title compound, C(13)H(15)NO(3), was synthesized by the Aldol reaction of isatin and 3-methyl­butan-2-one refluxing in methanol catalyzed by dimethyl­amine. The packing of the mol­ecules in the crystal structure features inter­molecular N—H⋯O and O—H⋯O hydrogen bonds.
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spelling pubmed-29772002010-12-30 3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one Chen, Gang Liu, Bin Tang, Ying Xu, Jingfang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(15)NO(3), was synthesized by the Aldol reaction of isatin and 3-methyl­butan-2-one refluxing in methanol catalyzed by dimethyl­amine. The packing of the mol­ecules in the crystal structure features inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2009-07-01 /pmc/articles/PMC2977200/ /pubmed/21583440 http://dx.doi.org/10.1107/S1600536809024611 Text en © Chen et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chen, Gang
Liu, Bin
Tang, Ying
Xu, Jingfang
3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
title 3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
title_full 3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
title_fullStr 3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
title_full_unstemmed 3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
title_short 3-Hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
title_sort 3-hydr­oxy-3-[(2-methyl­propano­yl)meth­yl]indolin-2-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977200/
https://www.ncbi.nlm.nih.gov/pubmed/21583440
http://dx.doi.org/10.1107/S1600536809024611
work_keys_str_mv AT chengang 3hydroxy32methylpropanoylmethylindolin2one
AT liubin 3hydroxy32methylpropanoylmethylindolin2one
AT tangying 3hydroxy32methylpropanoylmethylindolin2one
AT xujingfang 3hydroxy32methylpropanoylmethylindolin2one

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