N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea

The title compound, C(13)H(10)ClN(3)OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothio­cyanate at room temperature. The thio­urea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings, while the angle between the benz...

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Detalles Bibliográficos
Autores principales: Ding, Yu-Jie, Yao, Jian, Wu, Jian-Chao, Dong, Wen-Kui, Tong, Jun-Feng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977241/
https://www.ncbi.nlm.nih.gov/pubmed/21583593
http://dx.doi.org/10.1107/S1600536809027081
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author Ding, Yu-Jie
Yao, Jian
Wu, Jian-Chao
Dong, Wen-Kui
Tong, Jun-Feng
author_facet Ding, Yu-Jie
Yao, Jian
Wu, Jian-Chao
Dong, Wen-Kui
Tong, Jun-Feng
author_sort Ding, Yu-Jie
collection PubMed
description The title compound, C(13)H(10)ClN(3)OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothio­cyanate at room temperature. The thio­urea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings, while the angle between the benzene and pyridine rings is 8.91 (3)°. Inter­molecular hydrogen-bond inter­actions link neighbouring mol­ecules into an infinite supra­molecular structure.
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spelling pubmed-29772412010-12-30 N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea Ding, Yu-Jie Yao, Jian Wu, Jian-Chao Dong, Wen-Kui Tong, Jun-Feng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(10)ClN(3)OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothio­cyanate at room temperature. The thio­urea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings, while the angle between the benzene and pyridine rings is 8.91 (3)°. Inter­molecular hydrogen-bond inter­actions link neighbouring mol­ecules into an infinite supra­molecular structure. International Union of Crystallography 2009-07-18 /pmc/articles/PMC2977241/ /pubmed/21583593 http://dx.doi.org/10.1107/S1600536809027081 Text en © Ding et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ding, Yu-Jie
Yao, Jian
Wu, Jian-Chao
Dong, Wen-Kui
Tong, Jun-Feng
N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea
title N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea
title_full N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea
title_fullStr N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea
title_full_unstemmed N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea
title_short N-Benzoyl-N′-(2-chloro-3-pyrid­yl)thio­urea
title_sort n-benzoyl-n′-(2-chloro-3-pyrid­yl)thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977241/
https://www.ncbi.nlm.nih.gov/pubmed/21583593
http://dx.doi.org/10.1107/S1600536809027081
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