1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione

The title compound, C(10)H(12)N(2)O(2), was synthesized by cyclization of 3-(1-ethyl­pyrrole-2-carboxamido)propanoic acid in the presence of polyphospho­ric acid and diphospho­rus pentoxide. In the crystal structure, adjacent mol­ecules are linked by N—H⋯O hydrogen bonds, forming chains extending al...

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Detalles Bibliográficos
Autores principales: Li, Dong Dong, Tang, Gui Hong, Zeng, Xiang Chao, Xu, Xing Yan, Huang, Gang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977308/
https://www.ncbi.nlm.nih.gov/pubmed/21583611
http://dx.doi.org/10.1107/S1600536809027378
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author Li, Dong Dong
Tang, Gui Hong
Zeng, Xiang Chao
Xu, Xing Yan
Huang, Gang
author_facet Li, Dong Dong
Tang, Gui Hong
Zeng, Xiang Chao
Xu, Xing Yan
Huang, Gang
author_sort Li, Dong Dong
collection PubMed
description The title compound, C(10)H(12)N(2)O(2), was synthesized by cyclization of 3-(1-ethyl­pyrrole-2-carboxamido)propanoic acid in the presence of polyphospho­ric acid and diphospho­rus pentoxide. In the crystal structure, adjacent mol­ecules are linked by N—H⋯O hydrogen bonds, forming chains extending along the b axis.
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spelling pubmed-29773082010-12-30 1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione Li, Dong Dong Tang, Gui Hong Zeng, Xiang Chao Xu, Xing Yan Huang, Gang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(12)N(2)O(2), was synthesized by cyclization of 3-(1-ethyl­pyrrole-2-carboxamido)propanoic acid in the presence of polyphospho­ric acid and diphospho­rus pentoxide. In the crystal structure, adjacent mol­ecules are linked by N—H⋯O hydrogen bonds, forming chains extending along the b axis. International Union of Crystallography 2009-07-18 /pmc/articles/PMC2977308/ /pubmed/21583611 http://dx.doi.org/10.1107/S1600536809027378 Text en © Li et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Dong Dong
Tang, Gui Hong
Zeng, Xiang Chao
Xu, Xing Yan
Huang, Gang
1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione
title 1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione
title_full 1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione
title_fullStr 1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione
title_full_unstemmed 1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione
title_short 1-Ethyl-1H,6H-pyrrolo[2,3-c]azepine-4,8(5H,7H)-dione
title_sort 1-ethyl-1h,6h-pyrrolo[2,3-c]azepine-4,8(5h,7h)-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977308/
https://www.ncbi.nlm.nih.gov/pubmed/21583611
http://dx.doi.org/10.1107/S1600536809027378
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