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Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)

The hydro­thermal reaction of butane-1,2,3,4-tetra­carboxylic acid (H(4)butca), 4,4′-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O—H⋯N hydrogen-bonding and weak π–π stacking [centroid–centroid distance = 3.845...

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Detalles Bibliográficos
Autores principales: Zhang, Ning, Shi, Xue-Min, Shao, Min, Li, Ming-Xing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977318/
https://www.ncbi.nlm.nih.gov/pubmed/21583687
http://dx.doi.org/10.1107/S1600536809029237
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author Zhang, Ning
Shi, Xue-Min
Shao, Min
Li, Ming-Xing
author_facet Zhang, Ning
Shi, Xue-Min
Shao, Min
Li, Ming-Xing
author_sort Zhang, Ning
collection PubMed
description The hydro­thermal reaction of butane-1,2,3,4-tetra­carboxylic acid (H(4)butca), 4,4′-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O—H⋯N hydrogen-bonding and weak π–π stacking [centroid–centroid distance = 3.8459 (19) Å] inter­actions assemble the organic mol­ecules into a three-dimensional supra­molecular framework. C—H⋯O inter­actions are also present. The whole mol­ecule has inversion symmetry.
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spelling pubmed-29773182010-12-30 Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2) Zhang, Ning Shi, Xue-Min Shao, Min Li, Ming-Xing Acta Crystallogr Sect E Struct Rep Online Organic Papers The hydro­thermal reaction of butane-1,2,3,4-tetra­carboxylic acid (H(4)butca), 4,4′-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O—H⋯N hydrogen-bonding and weak π–π stacking [centroid–centroid distance = 3.8459 (19) Å] inter­actions assemble the organic mol­ecules into a three-dimensional supra­molecular framework. C—H⋯O inter­actions are also present. The whole mol­ecule has inversion symmetry. International Union of Crystallography 2009-07-29 /pmc/articles/PMC2977318/ /pubmed/21583687 http://dx.doi.org/10.1107/S1600536809029237 Text en © Zhang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Ning
Shi, Xue-Min
Shao, Min
Li, Ming-Xing
Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
title Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
title_full Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
title_fullStr Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
title_full_unstemmed Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
title_short Butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
title_sort butane-1,2,3,4-tetra­carboxylic acid–4,4′-bipyridine (1/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977318/
https://www.ncbi.nlm.nih.gov/pubmed/21583687
http://dx.doi.org/10.1107/S1600536809029237
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