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Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2)
The hydrothermal reaction of butane-1,2,3,4-tetracarboxylic acid (H(4)butca), 4,4′-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O—H⋯N hydrogen-bonding and weak π–π stacking [centroid–centroid distance = 3.845...
Autores principales: | , , , |
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977318/ https://www.ncbi.nlm.nih.gov/pubmed/21583687 http://dx.doi.org/10.1107/S1600536809029237 |
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author | Zhang, Ning Shi, Xue-Min Shao, Min Li, Ming-Xing |
author_facet | Zhang, Ning Shi, Xue-Min Shao, Min Li, Ming-Xing |
author_sort | Zhang, Ning |
collection | PubMed |
description | The hydrothermal reaction of butane-1,2,3,4-tetracarboxylic acid (H(4)butca), 4,4′-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O—H⋯N hydrogen-bonding and weak π–π stacking [centroid–centroid distance = 3.8459 (19) Å] interactions assemble the organic molecules into a three-dimensional supramolecular framework. C—H⋯O interactions are also present. The whole molecule has inversion symmetry. |
format | Text |
id | pubmed-2977318 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29773182010-12-30 Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) Zhang, Ning Shi, Xue-Min Shao, Min Li, Ming-Xing Acta Crystallogr Sect E Struct Rep Online Organic Papers The hydrothermal reaction of butane-1,2,3,4-tetracarboxylic acid (H(4)butca), 4,4′-bipyridine (bipy) and Mn(SO(4))(2)·H(2)O afforded a new co-crystal, C(8)H(10)O(8)·2C(10)H(8)N(2) or H(4)butca·2(bipy), in which strong O—H⋯N hydrogen-bonding and weak π–π stacking [centroid–centroid distance = 3.8459 (19) Å] interactions assemble the organic molecules into a three-dimensional supramolecular framework. C—H⋯O interactions are also present. The whole molecule has inversion symmetry. International Union of Crystallography 2009-07-29 /pmc/articles/PMC2977318/ /pubmed/21583687 http://dx.doi.org/10.1107/S1600536809029237 Text en © Zhang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Zhang, Ning Shi, Xue-Min Shao, Min Li, Ming-Xing Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
title | Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
title_full | Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
title_fullStr | Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
title_full_unstemmed | Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
title_short | Butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
title_sort | butane-1,2,3,4-tetracarboxylic acid–4,4′-bipyridine (1/2) |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977318/ https://www.ncbi.nlm.nih.gov/pubmed/21583687 http://dx.doi.org/10.1107/S1600536809029237 |
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