(E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate

The title compound, C(21)H(21)BrO(7)·C(2)H(6)O, was synthesized by the Claisen–Schimidt reaction of helicid (systematic name: 4-formyl­phenyl-β-d-allopyran­oside) with 4-bromo­aceto­phenone in ethanol. The pyran ring adopts a chair conformation. In the crystal structure, mol­ecules are linked into a...

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Detalles Bibliográficos
Autores principales: Yin, Xiu-Juan, Bai, Xue, Zheng, Lei, Li, Ying, Yin, Shu-Fan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977370/
https://www.ncbi.nlm.nih.gov/pubmed/21583708
http://dx.doi.org/10.1107/S1600536809029687
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author Yin, Xiu-Juan
Bai, Xue
Zheng, Lei
Li, Ying
Yin, Shu-Fan
author_facet Yin, Xiu-Juan
Bai, Xue
Zheng, Lei
Li, Ying
Yin, Shu-Fan
author_sort Yin, Xiu-Juan
collection PubMed
description The title compound, C(21)H(21)BrO(7)·C(2)H(6)O, was synthesized by the Claisen–Schimidt reaction of helicid (systematic name: 4-formyl­phenyl-β-d-allopyran­oside) with 4-bromo­aceto­phenone in ethanol. The pyran ring adopts a chair conformation. In the crystal structure, mol­ecules are linked into a three-dimensional network by inter­molecular O—H⋯O hydrogen bonds.
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spelling pubmed-29773702010-12-30 (E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate Yin, Xiu-Juan Bai, Xue Zheng, Lei Li, Ying Yin, Shu-Fan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(21)H(21)BrO(7)·C(2)H(6)O, was synthesized by the Claisen–Schimidt reaction of helicid (systematic name: 4-formyl­phenyl-β-d-allopyran­oside) with 4-bromo­aceto­phenone in ethanol. The pyran ring adopts a chair conformation. In the crystal structure, mol­ecules are linked into a three-dimensional network by inter­molecular O—H⋯O hydrogen bonds. International Union of Crystallography 2009-07-31 /pmc/articles/PMC2977370/ /pubmed/21583708 http://dx.doi.org/10.1107/S1600536809029687 Text en © Yin et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yin, Xiu-Juan
Bai, Xue
Zheng, Lei
Li, Ying
Yin, Shu-Fan
(E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
title (E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
title_full (E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
title_fullStr (E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
title_full_unstemmed (E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
title_short (E)-4-(β-d-Allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
title_sort (e)-4-(β-d-allopyran­os­yloxy)cinnamyl 4-bromo­phenyl ketone ethanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977370/
https://www.ncbi.nlm.nih.gov/pubmed/21583708
http://dx.doi.org/10.1107/S1600536809029687
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