1,2-Bis(3-hydroxy­benzyl­idene)diazane

The asymmetric unit of the title compound, C(14)H(12)N(2)O(2), which was synthesized unexpectedly by refluxing an ethano­lic solution of isonicotinic hydrazide and 3-hydroxy­benzaldehyde, contains one half-mol­ecule with the center of the N—N bond lying on a crystallographic center of inversion. In...

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Detalles Bibliográficos
Autores principales: Zhu, Ling, Zhao, Xin-Hua
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977383/
https://www.ncbi.nlm.nih.gov/pubmed/21583612
http://dx.doi.org/10.1107/S1600536809027652
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author Zhu, Ling
Zhao, Xin-Hua
author_facet Zhu, Ling
Zhao, Xin-Hua
author_sort Zhu, Ling
collection PubMed
description The asymmetric unit of the title compound, C(14)H(12)N(2)O(2), which was synthesized unexpectedly by refluxing an ethano­lic solution of isonicotinic hydrazide and 3-hydroxy­benzaldehyde, contains one half-mol­ecule with the center of the N—N bond lying on a crystallographic center of inversion. In the crystal structure, mol­ecules are linked by inter­molecular O—H⋯N hydrogen bonds into an infinite layer structure parallel to (110).
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spelling pubmed-29773832010-12-30 1,2-Bis(3-hydroxy­benzyl­idene)diazane Zhu, Ling Zhao, Xin-Hua Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(12)N(2)O(2), which was synthesized unexpectedly by refluxing an ethano­lic solution of isonicotinic hydrazide and 3-hydroxy­benzaldehyde, contains one half-mol­ecule with the center of the N—N bond lying on a crystallographic center of inversion. In the crystal structure, mol­ecules are linked by inter­molecular O—H⋯N hydrogen bonds into an infinite layer structure parallel to (110). International Union of Crystallography 2009-07-18 /pmc/articles/PMC2977383/ /pubmed/21583612 http://dx.doi.org/10.1107/S1600536809027652 Text en © Zhu and Zhao 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhu, Ling
Zhao, Xin-Hua
1,2-Bis(3-hydroxy­benzyl­idene)diazane
title 1,2-Bis(3-hydroxy­benzyl­idene)diazane
title_full 1,2-Bis(3-hydroxy­benzyl­idene)diazane
title_fullStr 1,2-Bis(3-hydroxy­benzyl­idene)diazane
title_full_unstemmed 1,2-Bis(3-hydroxy­benzyl­idene)diazane
title_short 1,2-Bis(3-hydroxy­benzyl­idene)diazane
title_sort 1,2-bis(3-hydroxy­benzyl­idene)diazane
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977383/
https://www.ncbi.nlm.nih.gov/pubmed/21583612
http://dx.doi.org/10.1107/S1600536809027652
work_keys_str_mv AT zhuling 12bis3hydroxybenzylidenediazane
AT zhaoxinhua 12bis3hydroxybenzylidenediazane

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