Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride

The crystal structure of the title compound, C(6)H(10)N(2) (2+)·2Cl(−), has been reported previously in the non-standard setting P2(1)/a [Genet (1965 ▶). Bull. Soc. Fr. Miner. Crist. 88, 463–470], with an R value of 0.16. The current redetermination improves significantly the precision of the geomet...

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Detalles Bibliográficos
Autores principales: Liang, Wen-Xian, Wang, Gang, Qu, Zhi-Rong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977397/
https://www.ncbi.nlm.nih.gov/pubmed/21583517
http://dx.doi.org/10.1107/S1600536809025859
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author Liang, Wen-Xian
Wang, Gang
Qu, Zhi-Rong
author_facet Liang, Wen-Xian
Wang, Gang
Qu, Zhi-Rong
author_sort Liang, Wen-Xian
collection PubMed
description The crystal structure of the title compound, C(6)H(10)N(2) (2+)·2Cl(−), has been reported previously in the non-standard setting P2(1)/a [Genet (1965 ▶). Bull. Soc. Fr. Miner. Crist. 88, 463–470], with an R value of 0.16. The current redetermination improves significantly the precision of the geometric parameters. In the crystal packing, cations and anions are linked by inter­molecular N—H⋯Cl and C—H⋯Cl hydrogen bonds into a three-dimensional network.
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spelling pubmed-29773972010-12-30 Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride Liang, Wen-Xian Wang, Gang Qu, Zhi-Rong Acta Crystallogr Sect E Struct Rep Online Organic Papers The crystal structure of the title compound, C(6)H(10)N(2) (2+)·2Cl(−), has been reported previously in the non-standard setting P2(1)/a [Genet (1965 ▶). Bull. Soc. Fr. Miner. Crist. 88, 463–470], with an R value of 0.16. The current redetermination improves significantly the precision of the geometric parameters. In the crystal packing, cations and anions are linked by inter­molecular N—H⋯Cl and C—H⋯Cl hydrogen bonds into a three-dimensional network. International Union of Crystallography 2009-07-11 /pmc/articles/PMC2977397/ /pubmed/21583517 http://dx.doi.org/10.1107/S1600536809025859 Text en © Liang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Liang, Wen-Xian
Wang, Gang
Qu, Zhi-Rong
Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
title Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
title_full Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
title_fullStr Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
title_full_unstemmed Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
title_short Redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
title_sort redetermination of 3-(ammonio­meth­yl)pyridinium dichloride
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977397/
https://www.ncbi.nlm.nih.gov/pubmed/21583517
http://dx.doi.org/10.1107/S1600536809025859
work_keys_str_mv AT liangwenxian redeterminationof3ammoniomethylpyridiniumdichloride
AT wanggang redeterminationof3ammoniomethylpyridiniumdichloride
AT quzhirong redeterminationof3ammoniomethylpyridiniumdichloride

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