4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione

The title compound, C(14)H(13)BrN(2)OS, was synthesized from the multicomponent reaction between thio­urea, 4-bromo­benzaldehyde and cyclo­hexane-1,3-dione. The crystal packing is stabilized by inter­molecular N—H⋯O, N—H⋯S, C—H⋯O and C—H⋯S hydrogen bonds. Br⋯O inter­actions [3.183 (3) Å] are also ob...

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Detalles Bibliográficos
Autores principales: Xie, Min, Deng, Changquan, Zheng, Jie, Zhu, Yulin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977462/
https://www.ncbi.nlm.nih.gov/pubmed/21583656
http://dx.doi.org/10.1107/S1600536809028761
Descripción
Sumario:The title compound, C(14)H(13)BrN(2)OS, was synthesized from the multicomponent reaction between thio­urea, 4-bromo­benzaldehyde and cyclo­hexane-1,3-dione. The crystal packing is stabilized by inter­molecular N—H⋯O, N—H⋯S, C—H⋯O and C—H⋯S hydrogen bonds. Br⋯O inter­actions [3.183 (3) Å] are also observed in the crystal structure.

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