4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione

The title compound, C(14)H(13)BrN(2)OS, was synthesized from the multicomponent reaction between thio­urea, 4-bromo­benzaldehyde and cyclo­hexane-1,3-dione. The crystal packing is stabilized by inter­molecular N—H⋯O, N—H⋯S, C—H⋯O and C—H⋯S hydrogen bonds. Br⋯O inter­actions [3.183 (3) Å] are also ob...

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Detalles Bibliográficos
Autores principales: Xie, Min, Deng, Changquan, Zheng, Jie, Zhu, Yulin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977462/
https://www.ncbi.nlm.nih.gov/pubmed/21583656
http://dx.doi.org/10.1107/S1600536809028761
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author Xie, Min
Deng, Changquan
Zheng, Jie
Zhu, Yulin
author_facet Xie, Min
Deng, Changquan
Zheng, Jie
Zhu, Yulin
author_sort Xie, Min
collection PubMed
description The title compound, C(14)H(13)BrN(2)OS, was synthesized from the multicomponent reaction between thio­urea, 4-bromo­benzaldehyde and cyclo­hexane-1,3-dione. The crystal packing is stabilized by inter­molecular N—H⋯O, N—H⋯S, C—H⋯O and C—H⋯S hydrogen bonds. Br⋯O inter­actions [3.183 (3) Å] are also observed in the crystal structure.
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spelling pubmed-29774622010-12-30 4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione Xie, Min Deng, Changquan Zheng, Jie Zhu, Yulin Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(13)BrN(2)OS, was synthesized from the multicomponent reaction between thio­urea, 4-bromo­benzaldehyde and cyclo­hexane-1,3-dione. The crystal packing is stabilized by inter­molecular N—H⋯O, N—H⋯S, C—H⋯O and C—H⋯S hydrogen bonds. Br⋯O inter­actions [3.183 (3) Å] are also observed in the crystal structure. International Union of Crystallography 2009-07-25 /pmc/articles/PMC2977462/ /pubmed/21583656 http://dx.doi.org/10.1107/S1600536809028761 Text en © Xie et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xie, Min
Deng, Changquan
Zheng, Jie
Zhu, Yulin
4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
title 4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
title_full 4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
title_fullStr 4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
title_full_unstemmed 4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
title_short 4-(4-Bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
title_sort 4-(4-bromo­phen­yl)-5-oxo-1,2,3,4,5,6,7,8-octa­hydro­quinazoline-2-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977462/
https://www.ncbi.nlm.nih.gov/pubmed/21583656
http://dx.doi.org/10.1107/S1600536809028761
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