2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)

The title compound, C(28)H(22)O(6)S(2)·2C(6)H(13)N·2H(2)O, was prepared by the reaction of a Wittig reagent and 2-formyl­benzene­sulfonic acid. The main molecule lies about an inversion centre at the midpoint of the C—C bond between the inner benzene rings. The mol­ecular conformation is stabilized...

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Detalles Bibliográficos
Autores principales: Li, Yu-Feng, Jian, Fang-Fang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977480/
https://www.ncbi.nlm.nih.gov/pubmed/21583614
http://dx.doi.org/10.1107/S1600536809026932
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author Li, Yu-Feng
Jian, Fang-Fang
author_facet Li, Yu-Feng
Jian, Fang-Fang
author_sort Li, Yu-Feng
collection PubMed
description The title compound, C(28)H(22)O(6)S(2)·2C(6)H(13)N·2H(2)O, was prepared by the reaction of a Wittig reagent and 2-formyl­benzene­sulfonic acid. The main molecule lies about an inversion centre at the midpoint of the C—C bond between the inner benzene rings. The mol­ecular conformation is stabilized by intramolecular hydrogen bonds. The crystal structure is further stabilized by O—H⋯O and N—H⋯O hydrogen-bonding inter­actions.
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spelling pubmed-29774802010-12-30 2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2) Li, Yu-Feng Jian, Fang-Fang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(28)H(22)O(6)S(2)·2C(6)H(13)N·2H(2)O, was prepared by the reaction of a Wittig reagent and 2-formyl­benzene­sulfonic acid. The main molecule lies about an inversion centre at the midpoint of the C—C bond between the inner benzene rings. The mol­ecular conformation is stabilized by intramolecular hydrogen bonds. The crystal structure is further stabilized by O—H⋯O and N—H⋯O hydrogen-bonding inter­actions. International Union of Crystallography 2009-07-18 /pmc/articles/PMC2977480/ /pubmed/21583614 http://dx.doi.org/10.1107/S1600536809026932 Text en © Li and Jian 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Yu-Feng
Jian, Fang-Fang
2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
title 2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
title_full 2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
title_fullStr 2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
title_full_unstemmed 2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
title_short 2,2′-[(Biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
title_sort 2,2′-[(biphenyl-4,4′-di­yl)di(ethene-1,2-di­yl)]dibenzene­sulfonic acid–4-methyl­piperidine–water (1/2/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977480/
https://www.ncbi.nlm.nih.gov/pubmed/21583614
http://dx.doi.org/10.1107/S1600536809026932
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