2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate

All the residues of the title compound, (C(5)H(6)N(3)O(2))[ReO(4)]·H(2)O, are located on general crystallographic positions. The 2-amino-5-nitro­pyridinium cation has a typical planar conformation with one of the nitro O atoms −0.058 (5) Å out of plane; the amine H atoms are also a little out of the...

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Autores principales: Rodrigues, V. H., Costa, M. M. R. R., Dekola, T., de Matos Gomes, E.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Metal-Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977490/
https://www.ncbi.nlm.nih.gov/pubmed/21583301
http://dx.doi.org/10.1107/S1600536809029365
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author Rodrigues, V. H.
Costa, M. M. R. R.
Dekola, T.
de Matos Gomes, E.
author_facet Rodrigues, V. H.
Costa, M. M. R. R.
Dekola, T.
de Matos Gomes, E.
author_sort Rodrigues, V. H.
collection PubMed
description All the residues of the title compound, (C(5)H(6)N(3)O(2))[ReO(4)]·H(2)O, are located on general crystallographic positions. The 2-amino-5-nitro­pyridinium cation has a typical planar conformation with one of the nitro O atoms −0.058 (5) Å out of plane; the amine H atoms are also a little out of the main ring plane towards the opposite side of the aforementioned O atom [by 0.02 (4) and 0.04 (4) Å]. The perrhenate anion is nearly ideally tetra­hedral. Three distinct N—H⋯O hydrogen bonds give rise to C(8) zigzag chains running along [100]. R (4) (4)(12) rings involving the two hydrogen bonds in which the water mol­ecules inter­act with the perrhenate anions are also present.
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spelling pubmed-29774902010-12-30 2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate Rodrigues, V. H. Costa, M. M. R. R. Dekola, T. de Matos Gomes, E. Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers All the residues of the title compound, (C(5)H(6)N(3)O(2))[ReO(4)]·H(2)O, are located on general crystallographic positions. The 2-amino-5-nitro­pyridinium cation has a typical planar conformation with one of the nitro O atoms −0.058 (5) Å out of plane; the amine H atoms are also a little out of the main ring plane towards the opposite side of the aforementioned O atom [by 0.02 (4) and 0.04 (4) Å]. The perrhenate anion is nearly ideally tetra­hedral. Three distinct N—H⋯O hydrogen bonds give rise to C(8) zigzag chains running along [100]. R (4) (4)(12) rings involving the two hydrogen bonds in which the water mol­ecules inter­act with the perrhenate anions are also present. International Union of Crystallography 2009-07-29 /pmc/articles/PMC2977490/ /pubmed/21583301 http://dx.doi.org/10.1107/S1600536809029365 Text en © Rodrigues et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Metal-Organic Papers
Rodrigues, V. H.
Costa, M. M. R. R.
Dekola, T.
de Matos Gomes, E.
2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate
title 2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate
title_full 2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate
title_fullStr 2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate
title_full_unstemmed 2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate
title_short 2-Amino-5-nitro­pyridinium tetraoxido­rhenate(VII) monohydrate
title_sort 2-amino-5-nitro­pyridinium tetraoxido­rhenate(vii) monohydrate
topic Metal-Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977490/
https://www.ncbi.nlm.nih.gov/pubmed/21583301
http://dx.doi.org/10.1107/S1600536809029365
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AT costammrr 2amino5nitropyridiniumtetraoxidorhenateviimonohydrate
AT dekolat 2amino5nitropyridiniumtetraoxidorhenateviimonohydrate
AT dematosgomese 2amino5nitropyridiniumtetraoxidorhenateviimonohydrate

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