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1,1-Bis[4-(trifluoromethyl)phenyl]germetane
The internal C—Ge—C bond angle in the germacyclobutane ring of the title compound, C(17)H(14)F(6)Ge or [Ge(C(3)H(6))(C(7)H(4)F(3))(2)], is 77.8 (3)°. The –CF(3) groups display rotational disorder [occupancies 0.604 (14):0.396 (14) and 0.410 (6):0.411 (6):0.179 (3)] and the germacyclobutane ring a...
Autores principales: | , , , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977636/ https://www.ncbi.nlm.nih.gov/pubmed/21583822 http://dx.doi.org/10.1107/S1600536809015268 |
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author | Huck, Lawrence A. Potter, Gregory D. Jenkins, Hilary A. Britten, James F. Leigh, William J. |
author_facet | Huck, Lawrence A. Potter, Gregory D. Jenkins, Hilary A. Britten, James F. Leigh, William J. |
author_sort | Huck, Lawrence A. |
collection | PubMed |
description | The internal C—Ge—C bond angle in the germacyclobutane ring of the title compound, C(17)H(14)F(6)Ge or [Ge(C(3)H(6))(C(7)H(4)F(3))(2)], is 77.8 (3)°. The –CF(3) groups display rotational disorder [occupancies 0.604 (14):0.396 (14) and 0.410 (6):0.411 (6):0.179 (3)] and the germacyclobutane ring also shows disorder [occupancies 0.604 (14):0.396 (14)]. |
format | Text |
id | pubmed-2977636 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29776362010-12-30 1,1-Bis[4-(trifluoromethyl)phenyl]germetane Huck, Lawrence A. Potter, Gregory D. Jenkins, Hilary A. Britten, James F. Leigh, William J. Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers The internal C—Ge—C bond angle in the germacyclobutane ring of the title compound, C(17)H(14)F(6)Ge or [Ge(C(3)H(6))(C(7)H(4)F(3))(2)], is 77.8 (3)°. The –CF(3) groups display rotational disorder [occupancies 0.604 (14):0.396 (14) and 0.410 (6):0.411 (6):0.179 (3)] and the germacyclobutane ring also shows disorder [occupancies 0.604 (14):0.396 (14)]. International Union of Crystallography 2009-04-30 /pmc/articles/PMC2977636/ /pubmed/21583822 http://dx.doi.org/10.1107/S1600536809015268 Text en © Huck et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Metal-Organic Papers Huck, Lawrence A. Potter, Gregory D. Jenkins, Hilary A. Britten, James F. Leigh, William J. 1,1-Bis[4-(trifluoromethyl)phenyl]germetane |
title | 1,1-Bis[4-(trifluoromethyl)phenyl]germetane |
title_full | 1,1-Bis[4-(trifluoromethyl)phenyl]germetane |
title_fullStr | 1,1-Bis[4-(trifluoromethyl)phenyl]germetane |
title_full_unstemmed | 1,1-Bis[4-(trifluoromethyl)phenyl]germetane |
title_short | 1,1-Bis[4-(trifluoromethyl)phenyl]germetane |
title_sort | 1,1-bis[4-(trifluoromethyl)phenyl]germetane |
topic | Metal-Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977636/ https://www.ncbi.nlm.nih.gov/pubmed/21583822 http://dx.doi.org/10.1107/S1600536809015268 |
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