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1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane

The inter­nal C—Ge—C bond angle in the germacyclo­butane ring of the title compound, C(17)H(14)F(6)Ge or [Ge(C(3)H(6))(C(7)H(4)F(3))(2)], is 77.8 (3)°. The –CF(3) groups display rotational disorder [occupancies 0.604 (14):0.396 (14) and 0.410 (6):0.411 (6):0.179 (3)] and the germacyclo­butane ring a...

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Detalles Bibliográficos
Autores principales: Huck, Lawrence A., Potter, Gregory D., Jenkins, Hilary A., Britten, James F., Leigh, William J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977636/
https://www.ncbi.nlm.nih.gov/pubmed/21583822
http://dx.doi.org/10.1107/S1600536809015268
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author Huck, Lawrence A.
Potter, Gregory D.
Jenkins, Hilary A.
Britten, James F.
Leigh, William J.
author_facet Huck, Lawrence A.
Potter, Gregory D.
Jenkins, Hilary A.
Britten, James F.
Leigh, William J.
author_sort Huck, Lawrence A.
collection PubMed
description The inter­nal C—Ge—C bond angle in the germacyclo­butane ring of the title compound, C(17)H(14)F(6)Ge or [Ge(C(3)H(6))(C(7)H(4)F(3))(2)], is 77.8 (3)°. The –CF(3) groups display rotational disorder [occupancies 0.604 (14):0.396 (14) and 0.410 (6):0.411 (6):0.179 (3)] and the germacyclo­butane ring also shows disorder [occupancies 0.604 (14):0.396 (14)].
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spelling pubmed-29776362010-12-30 1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane Huck, Lawrence A. Potter, Gregory D. Jenkins, Hilary A. Britten, James F. Leigh, William J. Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers The inter­nal C—Ge—C bond angle in the germacyclo­butane ring of the title compound, C(17)H(14)F(6)Ge or [Ge(C(3)H(6))(C(7)H(4)F(3))(2)], is 77.8 (3)°. The –CF(3) groups display rotational disorder [occupancies 0.604 (14):0.396 (14) and 0.410 (6):0.411 (6):0.179 (3)] and the germacyclo­butane ring also shows disorder [occupancies 0.604 (14):0.396 (14)]. International Union of Crystallography 2009-04-30 /pmc/articles/PMC2977636/ /pubmed/21583822 http://dx.doi.org/10.1107/S1600536809015268 Text en © Huck et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Metal-Organic Papers
Huck, Lawrence A.
Potter, Gregory D.
Jenkins, Hilary A.
Britten, James F.
Leigh, William J.
1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane
title 1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane
title_full 1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane
title_fullStr 1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane
title_full_unstemmed 1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane
title_short 1,1-Bis[4-(trifluoro­meth­yl)phen­yl]germetane
title_sort 1,1-bis[4-(trifluoro­meth­yl)phen­yl]germetane
topic Metal-Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977636/
https://www.ncbi.nlm.nih.gov/pubmed/21583822
http://dx.doi.org/10.1107/S1600536809015268
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