3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin

The title compound, 3-amino-5-methyl-5-(4-pyrid­yl)imid­azol­idine-2,4-dione, C(9)H(10)N(4)O(2), was obtained by reaction of 5-methyl-5-(4-pyrid­yl)hydantoin with hydrazine. It crystallizes as a racemate in the tetra­gonal space group I4(1)/a with one mol­ecule in the asymmetric unit. The dihedral a...

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Detalles Bibliográficos
Autores principales: Varbanov, Hristo, Buyukliev, Rossen, Bakalova, Adriana, Roller, Alexander
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977653/
https://www.ncbi.nlm.nih.gov/pubmed/21583996
http://dx.doi.org/10.1107/S1600536809011404
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author Varbanov, Hristo
Buyukliev, Rossen
Bakalova, Adriana
Roller, Alexander
author_facet Varbanov, Hristo
Buyukliev, Rossen
Bakalova, Adriana
Roller, Alexander
author_sort Varbanov, Hristo
collection PubMed
description The title compound, 3-amino-5-methyl-5-(4-pyrid­yl)imid­azol­idine-2,4-dione, C(9)H(10)N(4)O(2), was obtained by reaction of 5-methyl-5-(4-pyrid­yl)hydantoin with hydrazine. It crystallizes as a racemate in the tetra­gonal space group I4(1)/a with one mol­ecule in the asymmetric unit. The dihedral angle between the pyridine ring and the five-membered hydantoin ring is 47.99 (3)° In the crystal structure, mol­ecules are joined in a three-dimensional hydrogen-bonded network by N—H⋯N and N—H⋯O links.
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spelling pubmed-29776532010-12-30 3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin Varbanov, Hristo Buyukliev, Rossen Bakalova, Adriana Roller, Alexander Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, 3-amino-5-methyl-5-(4-pyrid­yl)imid­azol­idine-2,4-dione, C(9)H(10)N(4)O(2), was obtained by reaction of 5-methyl-5-(4-pyrid­yl)hydantoin with hydrazine. It crystallizes as a racemate in the tetra­gonal space group I4(1)/a with one mol­ecule in the asymmetric unit. The dihedral angle between the pyridine ring and the five-membered hydantoin ring is 47.99 (3)° In the crystal structure, mol­ecules are joined in a three-dimensional hydrogen-bonded network by N—H⋯N and N—H⋯O links. International Union of Crystallography 2009-04-02 /pmc/articles/PMC2977653/ /pubmed/21583996 http://dx.doi.org/10.1107/S1600536809011404 Text en © Varbanov et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Varbanov, Hristo
Buyukliev, Rossen
Bakalova, Adriana
Roller, Alexander
3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin
title 3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin
title_full 3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin
title_fullStr 3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin
title_full_unstemmed 3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin
title_short 3-Amino-5-methyl-5-(4-pyrid­yl)hydantoin
title_sort 3-amino-5-methyl-5-(4-pyrid­yl)hydantoin
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977653/
https://www.ncbi.nlm.nih.gov/pubmed/21583996
http://dx.doi.org/10.1107/S1600536809011404
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AT buyuklievrossen 3amino5methyl54pyridylhydantoin
AT bakalovaadriana 3amino5methyl54pyridylhydantoin
AT rolleralexander 3amino5methyl54pyridylhydantoin

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