5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine

The title compound, C(9)H(9)N(3)S, was synthesized by the reaction of 4-methyl-benzoic acid and thio­semicarbazide. The thia­diazol ring adopts a planar conformation and makes a dihedral angle of 31.19 (18)° with the phenyl ring. In the crystal, mol­ecules are linked by N—H⋯N hydrogen bonds....

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Detalles Bibliográficos
Autores principales: Guan, Jian-Ning, Wan, Rong, Wang, Yao, Han, Feng, Xu, Cheng-Zhen
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977673/
https://www.ncbi.nlm.nih.gov/pubmed/21584016
http://dx.doi.org/10.1107/S1600536809012434
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author Guan, Jian-Ning
Wan, Rong
Wang, Yao
Han, Feng
Xu, Cheng-Zhen
author_facet Guan, Jian-Ning
Wan, Rong
Wang, Yao
Han, Feng
Xu, Cheng-Zhen
author_sort Guan, Jian-Ning
collection PubMed
description The title compound, C(9)H(9)N(3)S, was synthesized by the reaction of 4-methyl-benzoic acid and thio­semicarbazide. The thia­diazol ring adopts a planar conformation and makes a dihedral angle of 31.19 (18)° with the phenyl ring. In the crystal, mol­ecules are linked by N—H⋯N hydrogen bonds.
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spelling pubmed-29776732010-12-30 5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine Guan, Jian-Ning Wan, Rong Wang, Yao Han, Feng Xu, Cheng-Zhen Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(9)H(9)N(3)S, was synthesized by the reaction of 4-methyl-benzoic acid and thio­semicarbazide. The thia­diazol ring adopts a planar conformation and makes a dihedral angle of 31.19 (18)° with the phenyl ring. In the crystal, mol­ecules are linked by N—H⋯N hydrogen bonds. International Union of Crystallography 2009-04-08 /pmc/articles/PMC2977673/ /pubmed/21584016 http://dx.doi.org/10.1107/S1600536809012434 Text en © Guan et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Guan, Jian-Ning
Wan, Rong
Wang, Yao
Han, Feng
Xu, Cheng-Zhen
5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine
title 5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine
title_full 5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine
title_fullStr 5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine
title_full_unstemmed 5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine
title_short 5-(4-Meth­ylphenyl)-1,3,4-thia­diazol-2-amine
title_sort 5-(4-meth­ylphenyl)-1,3,4-thia­diazol-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977673/
https://www.ncbi.nlm.nih.gov/pubmed/21584016
http://dx.doi.org/10.1107/S1600536809012434
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AT wanrong 54methylphenyl134thiadiazol2amine
AT wangyao 54methylphenyl134thiadiazol2amine
AT hanfeng 54methylphenyl134thiadiazol2amine
AT xuchengzhen 54methylphenyl134thiadiazol2amine

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