2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate

In the title compound, C(19)H(13)N(5)·3CH(4)O, the 2,6-bis­(2-benzimidazol­yl)pyridine mol­ecule is essentially planar with an r.m.s. deviation for all non-H atoms of 0.185 Å. The crystal structure is stabilized by inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds and weak π⋯π stacking inter­act...

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Detalles Bibliográficos
Autores principales: Chen, Ying, Guo, Jixi, Huang, Xingcai, Yun, Ruirui, Wu, Huilu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977700/
https://www.ncbi.nlm.nih.gov/pubmed/21583836
http://dx.doi.org/10.1107/S1600536809012574
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author Chen, Ying
Guo, Jixi
Huang, Xingcai
Yun, Ruirui
Wu, Huilu
author_facet Chen, Ying
Guo, Jixi
Huang, Xingcai
Yun, Ruirui
Wu, Huilu
author_sort Chen, Ying
collection PubMed
description In the title compound, C(19)H(13)N(5)·3CH(4)O, the 2,6-bis­(2-benzimidazol­yl)pyridine mol­ecule is essentially planar with an r.m.s. deviation for all non-H atoms of 0.185 Å. The crystal structure is stabilized by inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds and weak π⋯π stacking inter­actions with centroid–centroid distances of 3.6675 (16) and 3.6891 (15) Å. The atoms of one of the methanol solvent molecules are disordered over two sites with refined occupancies of 0.606(8) and 0.394(8).
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spelling pubmed-29777002010-12-30 2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate Chen, Ying Guo, Jixi Huang, Xingcai Yun, Ruirui Wu, Huilu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(19)H(13)N(5)·3CH(4)O, the 2,6-bis­(2-benzimidazol­yl)pyridine mol­ecule is essentially planar with an r.m.s. deviation for all non-H atoms of 0.185 Å. The crystal structure is stabilized by inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds and weak π⋯π stacking inter­actions with centroid–centroid distances of 3.6675 (16) and 3.6891 (15) Å. The atoms of one of the methanol solvent molecules are disordered over two sites with refined occupancies of 0.606(8) and 0.394(8). International Union of Crystallography 2009-04-10 /pmc/articles/PMC2977700/ /pubmed/21583836 http://dx.doi.org/10.1107/S1600536809012574 Text en © Chen et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chen, Ying
Guo, Jixi
Huang, Xingcai
Yun, Ruirui
Wu, Huilu
2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate
title 2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate
title_full 2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate
title_fullStr 2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate
title_full_unstemmed 2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate
title_short 2,6-Bis(1H-benzimidazol­-2-yl)pyridine methanol trisolvate
title_sort 2,6-bis(1h-benzimidazol­-2-yl)pyridine methanol trisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977700/
https://www.ncbi.nlm.nih.gov/pubmed/21583836
http://dx.doi.org/10.1107/S1600536809012574
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