5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine

The title compound, C(14)H(11)N(3)OS, was synthesized by the reaction of phenoxy­benzoic acid and thio­semicarbazide. The thia­diazole ring makes dihedral angles of 0.99 (16) and 86.53 (18)°, respectively, with the benzene and phenyl rings. The dihedral angle between the benzene and phenyl rings is...

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Detalles Bibliográficos
Autores principales: Wan, Rong, Wang, Yao, Han, Feng, Wang, Peng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977727/
https://www.ncbi.nlm.nih.gov/pubmed/21583863
http://dx.doi.org/10.1107/S1600536809013257
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author Wan, Rong
Wang, Yao
Han, Feng
Wang, Peng
author_facet Wan, Rong
Wang, Yao
Han, Feng
Wang, Peng
author_sort Wan, Rong
collection PubMed
description The title compound, C(14)H(11)N(3)OS, was synthesized by the reaction of phenoxy­benzoic acid and thio­semicarbazide. The thia­diazole ring makes dihedral angles of 0.99 (16) and 86.53 (18)°, respectively, with the benzene and phenyl rings. The dihedral angle between the benzene and phenyl rings is 87.17 (19)°. Intra­molecular C—H⋯S contacts are present. In the crystal, inter­molecular N—H⋯N hydrogen bonds link the mol­ecules.
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spelling pubmed-29777272010-12-30 5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine Wan, Rong Wang, Yao Han, Feng Wang, Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(11)N(3)OS, was synthesized by the reaction of phenoxy­benzoic acid and thio­semicarbazide. The thia­diazole ring makes dihedral angles of 0.99 (16) and 86.53 (18)°, respectively, with the benzene and phenyl rings. The dihedral angle between the benzene and phenyl rings is 87.17 (19)°. Intra­molecular C—H⋯S contacts are present. In the crystal, inter­molecular N—H⋯N hydrogen bonds link the mol­ecules. International Union of Crystallography 2009-04-18 /pmc/articles/PMC2977727/ /pubmed/21583863 http://dx.doi.org/10.1107/S1600536809013257 Text en © Wan et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wan, Rong
Wang, Yao
Han, Feng
Wang, Peng
5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
title 5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
title_full 5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
title_fullStr 5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
title_full_unstemmed 5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
title_short 5-(4-Phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
title_sort 5-(4-phenoxy­phen­yl)-1,3,4-thia­diazol-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977727/
https://www.ncbi.nlm.nih.gov/pubmed/21583863
http://dx.doi.org/10.1107/S1600536809013257
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AT wangpeng 54phenoxyphenyl134thiadiazol2amine

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