4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate

The crystal structure of the title compound, C(12)H(17)N(3)O(2) (+)·ClO(4) (−), consists of 4,4,5,5-tetra­methyl-2-(4-pyridinio)imidazoline-1-oxyl-3-oxide radical cations and perchlorate anions. Both the cation and the Cl atom of the anion are located on the same twofold rotation axis, and the cryst...

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Detalles Bibliográficos
Autores principales: Gao, Zhi-Yong, Chang, Jiu-Li, Xian, Dong, Jiang, Kai
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977742/
https://www.ncbi.nlm.nih.gov/pubmed/21583878
http://dx.doi.org/10.1107/S1600536809013531
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author Gao, Zhi-Yong
Chang, Jiu-Li
Xian, Dong
Jiang, Kai
author_facet Gao, Zhi-Yong
Chang, Jiu-Li
Xian, Dong
Jiang, Kai
author_sort Gao, Zhi-Yong
collection PubMed
description The crystal structure of the title compound, C(12)H(17)N(3)O(2) (+)·ClO(4) (−), consists of 4,4,5,5-tetra­methyl-2-(4-pyridinio)imidazoline-1-oxyl-3-oxide radical cations and perchlorate anions. Both the cation and the Cl atom of the anion are located on the same twofold rotation axis, and the crystal structure shows the average structure for the radical cation. The five-membered ring assumes a half-chair conformation. The cation links with the anion via N—H⋯O hydrogen bonding.
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spelling pubmed-29777422010-12-30 4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate Gao, Zhi-Yong Chang, Jiu-Li Xian, Dong Jiang, Kai Acta Crystallogr Sect E Struct Rep Online Organic Papers The crystal structure of the title compound, C(12)H(17)N(3)O(2) (+)·ClO(4) (−), consists of 4,4,5,5-tetra­methyl-2-(4-pyridinio)imidazoline-1-oxyl-3-oxide radical cations and perchlorate anions. Both the cation and the Cl atom of the anion are located on the same twofold rotation axis, and the crystal structure shows the average structure for the radical cation. The five-membered ring assumes a half-chair conformation. The cation links with the anion via N—H⋯O hydrogen bonding. International Union of Crystallography 2009-04-18 /pmc/articles/PMC2977742/ /pubmed/21583878 http://dx.doi.org/10.1107/S1600536809013531 Text en © Gao et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gao, Zhi-Yong
Chang, Jiu-Li
Xian, Dong
Jiang, Kai
4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
title 4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
title_full 4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
title_fullStr 4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
title_full_unstemmed 4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
title_short 4,4,5,5-Tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
title_sort 4,4,5,5-tetra­methyl-2-(4-pyridinio)-2-imidazoline-1-oxyl-3-oxide perchlorate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977742/
https://www.ncbi.nlm.nih.gov/pubmed/21583878
http://dx.doi.org/10.1107/S1600536809013531
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AT changjiuli 4455tetramethyl24pyridinio2imidazoline1oxyl3oxideperchlorate
AT xiandong 4455tetramethyl24pyridinio2imidazoline1oxyl3oxideperchlorate
AT jiangkai 4455tetramethyl24pyridinio2imidazoline1oxyl3oxideperchlorate

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