7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione

In the title compound, C(27)H(30)O(8), the cyclo­hexane ring is in a chair conformation, while the five-membered ring adopts an envelope conformation. The 1,3-dioxane ring is oriented with respect to the benzene rings at dihedral angles of 53.38 (3) and 55.31 (3)°, while the dihedral angle between t...

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Detalles Bibliográficos
Autores principales: Zhang, Jinpeng, Yan, Shu, Ding, Jie
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977755/
https://www.ncbi.nlm.nih.gov/pubmed/21583891
http://dx.doi.org/10.1107/S1600536809013658
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author Zhang, Jinpeng
Yan, Shu
Ding, Jie
author_facet Zhang, Jinpeng
Yan, Shu
Ding, Jie
author_sort Zhang, Jinpeng
collection PubMed
description In the title compound, C(27)H(30)O(8), the cyclo­hexane ring is in a chair conformation, while the five-membered ring adopts an envelope conformation. The 1,3-dioxane ring is oriented with respect to the benzene rings at dihedral angles of 53.38 (3) and 55.31 (3)°, while the dihedral angle between the benzene rings is 71.56 (3)°. In the crystal structure, inter­molecular C—H⋯O inter­actions link the mol­ecules into chains.
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spelling pubmed-29777552010-12-30 7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione Zhang, Jinpeng Yan, Shu Ding, Jie Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(27)H(30)O(8), the cyclo­hexane ring is in a chair conformation, while the five-membered ring adopts an envelope conformation. The 1,3-dioxane ring is oriented with respect to the benzene rings at dihedral angles of 53.38 (3) and 55.31 (3)°, while the dihedral angle between the benzene rings is 71.56 (3)°. In the crystal structure, inter­molecular C—H⋯O inter­actions link the mol­ecules into chains. International Union of Crystallography 2009-04-18 /pmc/articles/PMC2977755/ /pubmed/21583891 http://dx.doi.org/10.1107/S1600536809013658 Text en © Zhang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Jinpeng
Yan, Shu
Ding, Jie
7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
title 7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
title_full 7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
title_fullStr 7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
title_full_unstemmed 7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
title_short 7,14-Bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
title_sort 7,14-bis(4-methoxy­phen­yl)-11,11-dimethyl-1,4,10,12-tetra­oxa­dispiro­[4.2.5.2]penta­decane-9,13-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977755/
https://www.ncbi.nlm.nih.gov/pubmed/21583891
http://dx.doi.org/10.1107/S1600536809013658
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AT dingjie 714bis4methoxyphenyl1111dimethyl141012tetraoxadispiro4252pentadecane913dione

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