5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine

The title compound, C(7)H(6)N(4)S, was synthesized by reacting pyridine-4-carboxylic acid and thio­semicarbazide. The asymmetric unit contains two independent mol­ecules, which present different conformations, the dihedral angles between the thia­diazole and pyridine rings being 18.2 (2) and 30.3 (2...

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Detalles Bibliográficos
Autores principales: Wang, Yao, Wan, Rong, Han, Feng, Wang, Peng, Wang, Bin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977777/
https://www.ncbi.nlm.nih.gov/pubmed/21583913
http://dx.doi.org/10.1107/S1600536809014470
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author Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
Wang, Bin
author_facet Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
Wang, Bin
author_sort Wang, Yao
collection PubMed
description The title compound, C(7)H(6)N(4)S, was synthesized by reacting pyridine-4-carboxylic acid and thio­semicarbazide. The asymmetric unit contains two independent mol­ecules, which present different conformations, the dihedral angles between the thia­diazole and pyridine rings being 18.2 (2) and 30.3 (2)°. In the crystal, inter­molecular N—H⋯N hydrogen bonds involving the amine groups as donors link mol­ecules into a two-dimensional framework.
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spelling pubmed-29777772010-12-30 5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine Wang, Yao Wan, Rong Han, Feng Wang, Peng Wang, Bin Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(7)H(6)N(4)S, was synthesized by reacting pyridine-4-carboxylic acid and thio­semicarbazide. The asymmetric unit contains two independent mol­ecules, which present different conformations, the dihedral angles between the thia­diazole and pyridine rings being 18.2 (2) and 30.3 (2)°. In the crystal, inter­molecular N—H⋯N hydrogen bonds involving the amine groups as donors link mol­ecules into a two-dimensional framework. International Union of Crystallography 2009-04-25 /pmc/articles/PMC2977777/ /pubmed/21583913 http://dx.doi.org/10.1107/S1600536809014470 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
Wang, Bin
5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title 5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_full 5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_fullStr 5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_full_unstemmed 5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_short 5-(4-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_sort 5-(4-pyrid­yl)-1,3,4-thia­diazol-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977777/
https://www.ncbi.nlm.nih.gov/pubmed/21583913
http://dx.doi.org/10.1107/S1600536809014470
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AT wanrong 54pyridyl134thiadiazol2amine
AT hanfeng 54pyridyl134thiadiazol2amine
AT wangpeng 54pyridyl134thiadiazol2amine
AT wangbin 54pyridyl134thiadiazol2amine

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