Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate

In the title compound, C(22)H(26)N(2)O(5), the central 1,4-dihydro­pyrazine ring adopts a boat conformation, while the benzene ring and the two disordered components of the furan ring are inclined at angles of 77.9 (5) and 61.9 (7)°. Three of the C atoms of the furan ring are disordered over two pos...

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Detalles Bibliográficos
Autores principales: He, Jing-Yu, Tan, Zhi-Lin, Yan, Hong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977802/
https://www.ncbi.nlm.nih.gov/pubmed/21583939
http://dx.doi.org/10.1107/S1600536809013749
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author He, Jing-Yu
Tan, Zhi-Lin
Yan, Hong
author_facet He, Jing-Yu
Tan, Zhi-Lin
Yan, Hong
author_sort He, Jing-Yu
collection PubMed
description In the title compound, C(22)H(26)N(2)O(5), the central 1,4-dihydro­pyrazine ring adopts a boat conformation, while the benzene ring and the two disordered components of the furan ring are inclined at angles of 77.9 (5) and 61.9 (7)°. Three of the C atoms of the furan ring are disordered over two positions with occupancies of 0.655 (18) and 0.345 (18). In the crystal structure, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains propagating in [010].
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spelling pubmed-29778022010-12-30 Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate He, Jing-Yu Tan, Zhi-Lin Yan, Hong Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(22)H(26)N(2)O(5), the central 1,4-dihydro­pyrazine ring adopts a boat conformation, while the benzene ring and the two disordered components of the furan ring are inclined at angles of 77.9 (5) and 61.9 (7)°. Three of the C atoms of the furan ring are disordered over two positions with occupancies of 0.655 (18) and 0.345 (18). In the crystal structure, weak inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into chains propagating in [010]. International Union of Crystallography 2009-04-25 /pmc/articles/PMC2977802/ /pubmed/21583939 http://dx.doi.org/10.1107/S1600536809013749 Text en © He et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
He, Jing-Yu
Tan, Zhi-Lin
Yan, Hong
Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
title Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
title_full Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
title_fullStr Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
title_full_unstemmed Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
title_short Diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
title_sort diethyl 4-(4,5-dihydro­furan-2-yl)-3,5-di­methyl-1-phenyl-1,4-dihydro­pyrazine-2,6-dicarboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977802/
https://www.ncbi.nlm.nih.gov/pubmed/21583939
http://dx.doi.org/10.1107/S1600536809013749
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AT yanhong diethyl445dihydrofuran2yl35dimethyl1phenyl14dihydropyrazine26dicarboxylate

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