Methyl 9H-carbazole-9-acetate

The title compound, C(15)H(13)NO(2), was synthesized by N-alkyl­ation of methyl bromo­acetate with 9H-carbazole. The carbazole ring system is essentially planar (mean atomic deviation = 0.0346 Å) and makes a dihedral angle of 86.5 (7)° with the methyl acetate group. Weak inter­molecular C—H⋯O hydrog...

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Detalles Bibliográficos
Autores principales: He, Yong-Jun, Xie, Min-Hao, Zou, Pei, Liu, Ya-Ling, Wang, Hong-Yong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977808/
https://www.ncbi.nlm.nih.gov/pubmed/21583945
http://dx.doi.org/10.1107/S1600536809015141
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author He, Yong-Jun
Xie, Min-Hao
Zou, Pei
Liu, Ya-Ling
Wang, Hong-Yong
author_facet He, Yong-Jun
Xie, Min-Hao
Zou, Pei
Liu, Ya-Ling
Wang, Hong-Yong
author_sort He, Yong-Jun
collection PubMed
description The title compound, C(15)H(13)NO(2), was synthesized by N-alkyl­ation of methyl bromo­acetate with 9H-carbazole. The carbazole ring system is essentially planar (mean atomic deviation = 0.0346 Å) and makes a dihedral angle of 86.5 (7)° with the methyl acetate group. Weak inter­molecular C—H⋯O hydrogen bonding is present in the crystal structure.
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spelling pubmed-29778082010-12-30 Methyl 9H-carbazole-9-acetate He, Yong-Jun Xie, Min-Hao Zou, Pei Liu, Ya-Ling Wang, Hong-Yong Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(13)NO(2), was synthesized by N-alkyl­ation of methyl bromo­acetate with 9H-carbazole. The carbazole ring system is essentially planar (mean atomic deviation = 0.0346 Å) and makes a dihedral angle of 86.5 (7)° with the methyl acetate group. Weak inter­molecular C—H⋯O hydrogen bonding is present in the crystal structure. International Union of Crystallography 2009-04-25 /pmc/articles/PMC2977808/ /pubmed/21583945 http://dx.doi.org/10.1107/S1600536809015141 Text en © He et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
He, Yong-Jun
Xie, Min-Hao
Zou, Pei
Liu, Ya-Ling
Wang, Hong-Yong
Methyl 9H-carbazole-9-acetate
title Methyl 9H-carbazole-9-acetate
title_full Methyl 9H-carbazole-9-acetate
title_fullStr Methyl 9H-carbazole-9-acetate
title_full_unstemmed Methyl 9H-carbazole-9-acetate
title_short Methyl 9H-carbazole-9-acetate
title_sort methyl 9h-carbazole-9-acetate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2977808/
https://www.ncbi.nlm.nih.gov/pubmed/21583945
http://dx.doi.org/10.1107/S1600536809015141
work_keys_str_mv AT heyongjun methyl9hcarbazole9acetate
AT xieminhao methyl9hcarbazole9acetate
AT zoupei methyl9hcarbazole9acetate
AT liuyaling methyl9hcarbazole9acetate
AT wanghongyong methyl9hcarbazole9acetate

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