2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate

The asymmetric unit of the title compound, C(12)H(10)N(4)O(2)Se(2)·2C(3)H(7)NO, contains two solvent mol­ecules and two half mol­ecules of the dinicotinamide, each of which sits on a center of symmetry passing through the middle of the Se—Se bond. In each mol­ecule, the two pyridyl groups and disele...

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Detalles Bibliográficos
Autores principales: Feng, Aixia, Xu, Ying, Wei, Xuehong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979017/
https://www.ncbi.nlm.nih.gov/pubmed/21579243
http://dx.doi.org/10.1107/S1600536810015047
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author Feng, Aixia
Xu, Ying
Wei, Xuehong
author_facet Feng, Aixia
Xu, Ying
Wei, Xuehong
author_sort Feng, Aixia
collection PubMed
description The asymmetric unit of the title compound, C(12)H(10)N(4)O(2)Se(2)·2C(3)H(7)NO, contains two solvent mol­ecules and two half mol­ecules of the dinicotinamide, each of which sits on a center of symmetry passing through the middle of the Se—Se bond. In each mol­ecule, the two pyridyl groups and diseleno group are approximately coplanar (r.m.s. deviations from planarity for all non-H atoms = 0.011 and 0.008 Å in the two mol­ecules). Inter­molecular N—H⋯O hydrogen bonds stablilize the crystal packing.
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spelling pubmed-29790172010-12-30 2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate Feng, Aixia Xu, Ying Wei, Xuehong Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(12)H(10)N(4)O(2)Se(2)·2C(3)H(7)NO, contains two solvent mol­ecules and two half mol­ecules of the dinicotinamide, each of which sits on a center of symmetry passing through the middle of the Se—Se bond. In each mol­ecule, the two pyridyl groups and diseleno group are approximately coplanar (r.m.s. deviations from planarity for all non-H atoms = 0.011 and 0.008 Å in the two mol­ecules). Inter­molecular N—H⋯O hydrogen bonds stablilize the crystal packing. International Union of Crystallography 2010-04-30 /pmc/articles/PMC2979017/ /pubmed/21579243 http://dx.doi.org/10.1107/S1600536810015047 Text en © Feng et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Feng, Aixia
Xu, Ying
Wei, Xuehong
2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate
title 2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate
title_full 2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate
title_fullStr 2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate
title_full_unstemmed 2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate
title_short 2,2′-(Diselane-1,2-di­yl)dinicotinamide N,N′-dimethyl­formamide disolvate
title_sort 2,2′-(diselane-1,2-di­yl)dinicotinamide n,n′-dimethyl­formamide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979017/
https://www.ncbi.nlm.nih.gov/pubmed/21579243
http://dx.doi.org/10.1107/S1600536810015047
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