Bis[4-(4-chloro­phen­yl)-4-hydroxy­piperidinium] dipicrate dimethyl sulfoxide solvate

The asymmetric unit of the title salt solvate, 2C(11)H(15)ClNO(+)·2C(6)H(2)N(3)O(7) (−)·C(2)H(6)OS, contains two crystallographically independent 4-(4-chloro­phen­yl)-4-hydroxy­piperidinium cations, two picrate anions and a dimethyl sulfoxide solvent mol­ecule. In each cation, the piperidinium ring...

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Detalles Bibliográficos
Autores principales: Fun, Hoong-Kun, Hemamalini, Madhukar, Siddaraju, B. P., Yathirajan, H. S., Narayana, B.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979285/
https://www.ncbi.nlm.nih.gov/pubmed/21579241
http://dx.doi.org/10.1107/S1600536810015187
Descripción
Sumario:The asymmetric unit of the title salt solvate, 2C(11)H(15)ClNO(+)·2C(6)H(2)N(3)O(7) (−)·C(2)H(6)OS, contains two crystallographically independent 4-(4-chloro­phen­yl)-4-hydroxy­piperidinium cations, two picrate anions and a dimethyl sulfoxide solvent mol­ecule. In each cation, the piperidinium ring adopts a chair conformation. In the crystal structure, the cations, anions and solvent mol­ecules are connected by inter­molecular O—H⋯O, N—H⋯O and C—H⋯O hydrogen bonds, forming a three-dimensional network.

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