Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph

In the title compound, C(10)H(9)NO(5)S, the fused ring system and the planar (r.m.s. deviation = 0.0037 Å) methoxy­carbonyl­methyl side chain form a dihedral angle of 84.67 (10)°. The crystal structure is stabilized by inter­molecular C—H⋯O hydrogen bonds. A triclinic polymorph of the title compound...

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Detalles Bibliográficos
Autores principales: Zia-ur-Rehman, Muhammad, Arshad, Muhammad Nadeem, Mubarak, Shafaq, Khan, Islam Ullah
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979295/
https://www.ncbi.nlm.nih.gov/pubmed/21579092
http://dx.doi.org/10.1107/S1600536810012006
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author Zia-ur-Rehman, Muhammad
Arshad, Muhammad Nadeem
Mubarak, Shafaq
Khan, Islam Ullah
author_facet Zia-ur-Rehman, Muhammad
Arshad, Muhammad Nadeem
Mubarak, Shafaq
Khan, Islam Ullah
author_sort Zia-ur-Rehman, Muhammad
collection PubMed
description In the title compound, C(10)H(9)NO(5)S, the fused ring system and the planar (r.m.s. deviation = 0.0037 Å) methoxy­carbonyl­methyl side chain form a dihedral angle of 84.67 (10)°. The crystal structure is stabilized by inter­molecular C—H⋯O hydrogen bonds. A triclinic polymorph of the title compound is already known [Siddiqui et al. (2008 ▶). Acta Cryst. E64, o859].
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spelling pubmed-29792952010-12-30 Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph Zia-ur-Rehman, Muhammad Arshad, Muhammad Nadeem Mubarak, Shafaq Khan, Islam Ullah Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(10)H(9)NO(5)S, the fused ring system and the planar (r.m.s. deviation = 0.0037 Å) methoxy­carbonyl­methyl side chain form a dihedral angle of 84.67 (10)°. The crystal structure is stabilized by inter­molecular C—H⋯O hydrogen bonds. A triclinic polymorph of the title compound is already known [Siddiqui et al. (2008 ▶). Acta Cryst. E64, o859]. International Union of Crystallography 2010-04-10 /pmc/articles/PMC2979295/ /pubmed/21579092 http://dx.doi.org/10.1107/S1600536810012006 Text en © Zia-ur-Rehman et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zia-ur-Rehman, Muhammad
Arshad, Muhammad Nadeem
Mubarak, Shafaq
Khan, Islam Ullah
Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
title Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
title_full Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
title_fullStr Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
title_full_unstemmed Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
title_short Methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
title_sort methyl 2-(1,1,3-trioxo-2,3-dihydro-1,2-benzothia­zol-2-yl)acetate: a monoclinic polymorph
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979295/
https://www.ncbi.nlm.nih.gov/pubmed/21579092
http://dx.doi.org/10.1107/S1600536810012006
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AT mubarakshafaq methyl2113trioxo23dihydro12benzothiazol2ylacetateamonoclinicpolymorph
AT khanislamullah methyl2113trioxo23dihydro12benzothiazol2ylacetateamonoclinicpolymorph

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