(4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone

In the title compound, C(18)H(11)Br(2)ClO(3), an intra­molecular O—H⋯O=C hydrogen bond occurs, forming a six-membered ring. The naphthalene ring system and the benzene ring make a dihedral angle of 57.36 (9)°. The central carbonyl C—(C=O)—C group is twisted away from the naphthalene ring system and...

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Autores principales: Mitsui, Ryosuke, Watanabe, Shoji, Nagasawa, Atsushi, Okamoto, Akiko, Yonezawa, Noriyuki
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979364/
https://www.ncbi.nlm.nih.gov/pubmed/21579400
http://dx.doi.org/10.1107/S1600536810015527
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author Mitsui, Ryosuke
Watanabe, Shoji
Nagasawa, Atsushi
Okamoto, Akiko
Yonezawa, Noriyuki
author_facet Mitsui, Ryosuke
Watanabe, Shoji
Nagasawa, Atsushi
Okamoto, Akiko
Yonezawa, Noriyuki
author_sort Mitsui, Ryosuke
collection PubMed
description In the title compound, C(18)H(11)Br(2)ClO(3), an intra­molecular O—H⋯O=C hydrogen bond occurs, forming a six-membered ring. The naphthalene ring system and the benzene ring make a dihedral angle of 57.36 (9)°. The central carbonyl C—(C=O)—C group is twisted away from the naphthalene ring system and the benzene ring by 18.61 (15) and 26.25 (16)°, respectively. In the crystal structure, two inter­molecular Br⋯Cl close contacts [3.4927 (7) and 3.4325 (7) Å] are observed.
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spelling pubmed-29793642010-12-30 (4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone Mitsui, Ryosuke Watanabe, Shoji Nagasawa, Atsushi Okamoto, Akiko Yonezawa, Noriyuki Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(18)H(11)Br(2)ClO(3), an intra­molecular O—H⋯O=C hydrogen bond occurs, forming a six-membered ring. The naphthalene ring system and the benzene ring make a dihedral angle of 57.36 (9)°. The central carbonyl C—(C=O)—C group is twisted away from the naphthalene ring system and the benzene ring by 18.61 (15) and 26.25 (16)°, respectively. In the crystal structure, two inter­molecular Br⋯Cl close contacts [3.4927 (7) and 3.4325 (7) Å] are observed. International Union of Crystallography 2010-05-08 /pmc/articles/PMC2979364/ /pubmed/21579400 http://dx.doi.org/10.1107/S1600536810015527 Text en © Mitsui et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Mitsui, Ryosuke
Watanabe, Shoji
Nagasawa, Atsushi
Okamoto, Akiko
Yonezawa, Noriyuki
(4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
title (4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
title_full (4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
title_fullStr (4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
title_full_unstemmed (4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
title_short (4-Chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
title_sort (4-chloro­phen­yl)(3,8-dibromo-2-hydr­oxy-7-meth­oxy-1-naphth­yl)methanone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979364/
https://www.ncbi.nlm.nih.gov/pubmed/21579400
http://dx.doi.org/10.1107/S1600536810015527
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AT yonezawanoriyuki 4chlorophenyl38dibromo2hydroxy7methoxy1naphthylmethanone

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