2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)

In the title 2:1 adduct, C(14)H(10)O(4)S(2)·0.5C(10)H(8)N(2)O(2), which arose from an unexpected oxidation of a precursor, the dihedral angle between the aromatic rings in the disulfide is 82.51 (11)°. In the crystal, the molecules are linked by O—H⋯O, O—H⋯N and C—H⋯O interactions, generating sheets...

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Detalles Bibliográficos
Autores principales: Moreno-Fuquen, Rodolfo, Ellena, Javier, De Simone, Carlos A., Ribeiro, Leandro, De Almeida Santos, Regina Helena
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979473/
https://www.ncbi.nlm.nih.gov/pubmed/21579515
http://dx.doi.org/10.1107/S1600536810018775
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author Moreno-Fuquen, Rodolfo
Ellena, Javier
De Simone, Carlos A.
Ribeiro, Leandro
De Almeida Santos, Regina Helena
author_facet Moreno-Fuquen, Rodolfo
Ellena, Javier
De Simone, Carlos A.
Ribeiro, Leandro
De Almeida Santos, Regina Helena
author_sort Moreno-Fuquen, Rodolfo
collection PubMed
description In the title 2:1 adduct, C(14)H(10)O(4)S(2)·0.5C(10)H(8)N(2)O(2), which arose from an unexpected oxidation of a precursor, the dihedral angle between the aromatic rings in the disulfide is 82.51 (11)°. In the crystal, the molecules are linked by O—H⋯O, O—H⋯N and C—H⋯O interactions, generating sheets.
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spelling pubmed-29794732010-12-30 2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2) Moreno-Fuquen, Rodolfo Ellena, Javier De Simone, Carlos A. Ribeiro, Leandro De Almeida Santos, Regina Helena Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title 2:1 adduct, C(14)H(10)O(4)S(2)·0.5C(10)H(8)N(2)O(2), which arose from an unexpected oxidation of a precursor, the dihedral angle between the aromatic rings in the disulfide is 82.51 (11)°. In the crystal, the molecules are linked by O—H⋯O, O—H⋯N and C—H⋯O interactions, generating sheets. International Union of Crystallography 2010-05-26 /pmc/articles/PMC2979473/ /pubmed/21579515 http://dx.doi.org/10.1107/S1600536810018775 Text en © Moreno-Fuquen et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Moreno-Fuquen, Rodolfo
Ellena, Javier
De Simone, Carlos A.
Ribeiro, Leandro
De Almeida Santos, Regina Helena
2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)
title 2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)
title_full 2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)
title_fullStr 2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)
title_full_unstemmed 2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)
title_short 2-[(2-Carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl N,N′-dioxide (1/2)
title_sort 2-[(2-carboxy­phen­yl)disulfan­yl]benzoic acid–4,4′-bipyridyl n,n′-dioxide (1/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979473/
https://www.ncbi.nlm.nih.gov/pubmed/21579515
http://dx.doi.org/10.1107/S1600536810018775
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