4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione

The title compound, C(13)H(20)O(3)S(5), is bis­ected by a crystallographic twofold rotation axis, which relates the two halves of the mol­ecule to one another: one S, one C and one O atom lie on the axis. The thione S atom lies in the plane of the five-membered rings with an r.m.s. deviation of 0.00...

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Detalles Bibliográficos
Autores principales: Hou, Rui-Bin, Li, Bao, Yin, Bing-Zhu, Wu, Li-Xin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979504/
https://www.ncbi.nlm.nih.gov/pubmed/21579425
http://dx.doi.org/10.1107/S1600536810016946
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author Hou, Rui-Bin
Li, Bao
Yin, Bing-Zhu
Wu, Li-Xin
author_facet Hou, Rui-Bin
Li, Bao
Yin, Bing-Zhu
Wu, Li-Xin
author_sort Hou, Rui-Bin
collection PubMed
description The title compound, C(13)H(20)O(3)S(5), is bis­ected by a crystallographic twofold rotation axis, which relates the two halves of the mol­ecule to one another: one S, one C and one O atom lie on the axis. The thione S atom lies in the plane of the five-membered rings with an r.m.s. deviation of 0.0042 (5) Å. Parts of the 17-membered macrocycle were refined using a two-part disorder model [occupancies of 0.553 (14) and 0.447 (14)]. There are no noteworthy inter­molecular inter­actions.
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spelling pubmed-29795042010-12-30 4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione Hou, Rui-Bin Li, Bao Yin, Bing-Zhu Wu, Li-Xin Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(20)O(3)S(5), is bis­ected by a crystallographic twofold rotation axis, which relates the two halves of the mol­ecule to one another: one S, one C and one O atom lie on the axis. The thione S atom lies in the plane of the five-membered rings with an r.m.s. deviation of 0.0042 (5) Å. Parts of the 17-membered macrocycle were refined using a two-part disorder model [occupancies of 0.553 (14) and 0.447 (14)]. There are no noteworthy inter­molecular inter­actions. International Union of Crystallography 2010-05-15 /pmc/articles/PMC2979504/ /pubmed/21579425 http://dx.doi.org/10.1107/S1600536810016946 Text en © Hou et al. 2010 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hou, Rui-Bin
Li, Bao
Yin, Bing-Zhu
Wu, Li-Xin
4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
title 4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
title_full 4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
title_fullStr 4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
title_full_unstemmed 4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
title_short 4,6,7,9,10,12,13,15,16,18-Decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
title_sort 4,6,7,9,10,12,13,15,16,18-decahydro-1,3-dithiolo[4,5-l][1,4,7,10,15]trioxadithia­cyclo­hepta­decine-2-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2979504/
https://www.ncbi.nlm.nih.gov/pubmed/21579425
http://dx.doi.org/10.1107/S1600536810016946
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